2K9E
NMR Solution Structure for ShK-192: A Potent KV1.3-Specific Immunosuppressive Polypeptide
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | DRX | Bruker DRX | 600 |
| 2 | Bruker | AMX | Bruker AMX | 500 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 2D 1H-15N HSQC |
| 2 | 1 | 1 | 2D 1H-13C HSQC |
| 3 | 1 | 1 | 2D 1H-1H TOCSY |
| 4 | 2 | 2 | 2D 1H-1H TOCSY |
| 5 | 2 | 2 | 2D 1H-13C HSQC |
| 6 | 1 | 1 | 2D 1H-1H COSY |
| 7 | 1 | 1 | 2D 1H-1H NOESY |
| 8 | 2 | 2 | 2D 1H-1H NOESY |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 4.79 | ambient | 293 |
| 2 | 4.1 | ambient | 278 |
Conformers
| Conformers Calculated Total Number | 50 |
| Conformers Submitted Total Number | 20 |
