2JLR
Dengue virus 4 NS3 helicase in complex with AMPPNP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 100 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 52.632, 88.678, 54.698 |
| Unit cell angles | 90.00, 105.90, 90.00 |
Refinement procedure
| Resolution | 19.650 - 2.000 |
| R-factor | 0.20375 |
| Rwork | 0.201 |
| R-free | 0.25072 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2jlq |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.506 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 26.500 | 2.000 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.120 | 0.700 |
| Number of reflections | 34139 | |
| <I/σ(I)> | 11.1 | 1.3 |
| Completeness [%] | 93.6 | 79.9 |
| Redundancy | 4.1 | 3.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
