2JHT
CRYSTAL STRUCTURE OF RHOGDI K135T,K138T,K141T MUTANT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-04-19 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 190.832, 34.022, 103.940 |
Unit cell angles | 90.00, 115.59, 90.00 |
Refinement procedure
Resolution | 93.660 - 1.880 |
R-factor | 0.223 |
Rwork | 0.222 |
R-free | 0.25900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2bxw |
RMSD bond length | 0.020 |
RMSD bond angle | 1.845 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.130 | 0.260 |
Number of reflections | 44864 | |
<I/σ(I)> | 14.6 | 3.6 |
Completeness [%] | 91.5 | 64.4 |
Redundancy | 4.8 | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 35% PEG 4000 0.2 M LITHIUM SULFATE 0.1M TRIS PH 8.5 |