2JDR
STRUCTURE OF PKB-BETA (AKT2) COMPLEXED WITH THE INHIBITOR A-443654
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 44.927, 60.994, 124.963 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 54.810 - 2.300 |
R-factor | 0.196 |
Rwork | 0.193 |
R-free | 0.25200 |
Structure solution method | OTHER |
RMSD bond length | 0.013 |
RMSD bond angle | 1.382 |
Refinement software | REFMAC (5.2.0019F) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 55.000 |
High resolution limit [Å] | 2.300 |
Rmerge | 0.080 |
Number of reflections | 14109 |
<I/σ(I)> | 6.5 |
Completeness [%] | 95.0 |
Redundancy | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |