2JB6
Fab fragment in complex with small molecule hapten, crystal form-2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-01-21 |
Detector | MARRESEARCH |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 77.028, 77.028, 379.128 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.400 - 2.850 |
R-factor | 0.231 |
Rwork | 0.229 |
R-free | 0.28200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2jb5 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.283 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.900 | 2.900 |
High resolution limit [Å] | 2.850 | 2.850 |
Rmerge | 0.100 | 0.390 |
Number of reflections | 27756 | |
<I/σ(I)> | 15.6 | 3.5 |
Completeness [%] | 98.7 | 78.8 |
Redundancy | 5.7 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4 | 2.6-2.7M AMMONIUM SULPHATE, 5% PEG400, 0.1M SODIUM CITRATE PH 4. ADDITIONAL 10% GLYCEROL AS CRYO BUFFER. |