2EA2
h-MetAP2 complexed with A773812
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2002-11-12 |
Detector | MAR CCD 130 mm |
Wavelength(s) | 1.54 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 89.721, 99.060, 100.855 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 16.910 - 2.500 |
R-factor | 0.203 |
Rwork | 0.191 |
R-free | 0.25500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1yw7 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.300 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | CNX (2002) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 15352 | |
<I/σ(I)> | 15.3 | 6.2 |
Completeness [%] | 96.9 | 77.2 |
Redundancy | 6.5 | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 277 | 20-30 % isopropanol, 0.1M Na citrate, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |