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2BRQ

Crystal structure of the filamin A repeat 21 complexed with the integrin beta7 cytoplasmic tail peptide

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-3
Synchrotron siteESRF
BeamlineID14-3
Temperature [K]100
Detector technologyCCD
Collection date2005-02-17
DetectorMARRESEARCH MAR165
Spacegroup nameP 1 21 1
Unit cell lengths41.970, 60.000, 51.570
Unit cell angles90.00, 110.17, 90.00
Refinement procedure
Resolution37.680 - 2.100
R-factor0.197
Rwork0.192
R-free0.24300
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1v05
RMSD bond length0.014
RMSD bond angle1.465
Data reduction softwareXDS
Phasing softwarePHASER
Refinement softwareREFMAC (5.2.0005)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]37.6802.100
High resolution limit [Å]2.0002.000
Rmerge0.0700.050
Number of reflections13748
<I/σ(I)>17.65
Completeness [%]96.996.1
Redundancy5.25.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
15.51.26 M SODIUM CITRATE, 0.1 M CITRIC ACID PH 5.5

222036

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