2JLX
Dengue virus 4 NS3 helicase in complex with ssRNA and ADP-Vanadate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 132.537, 105.207, 72.352 |
Unit cell angles | 90.00, 117.62, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.200 |
R-factor | 0.19819 |
Rwork | 0.196 |
R-free | 0.24506 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2jlu |
RMSD bond length | 0.009 |
RMSD bond angle | 1.223 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 78.300 | 2.300 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.100 | 0.500 |
Number of reflections | 127207 | |
<I/σ(I)> | 11.6 | 2.7 |
Completeness [%] | 98.8 | 99.7 |
Redundancy | 2.9 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |