2JLR
Dengue virus 4 NS3 helicase in complex with AMPPNP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 100 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 52.632, 88.678, 54.698 |
Unit cell angles | 90.00, 105.90, 90.00 |
Refinement procedure
Resolution | 19.650 - 2.000 |
R-factor | 0.20375 |
Rwork | 0.201 |
R-free | 0.25072 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2jlq |
RMSD bond length | 0.003 |
RMSD bond angle | 0.506 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 26.500 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.120 | 0.700 |
Number of reflections | 34139 | |
<I/σ(I)> | 11.1 | 1.3 |
Completeness [%] | 93.6 | 79.9 |
Redundancy | 4.1 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |