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2C9W

CRYSTAL STRUCTURE OF SOCS-2 IN COMPLEX WITH ELONGIN-B AND ELONGIN-C AT 1.9A RESOLUTION

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X10SA
Synchrotron siteSLS
BeamlineX10SA
Temperature [K]100
Detector technologyCCD
Collection date2005-11-18
DetectorMARRESEARCH
Spacegroup nameP 32 2 1
Unit cell lengths105.290, 105.290, 70.200
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution91.290 - 1.900
R-factor0.187
Rwork0.185
R-free0.22500
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)PDB ENTRIES 1O4H 1lm8
RMSD bond length0.010
RMSD bond angle1.209
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwarePHASER
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]38.2502.000
High resolution limit [Å]1.9001.900
Rmerge0.0730.310
Number of reflections395240
<I/σ(I)>28.93.29
Completeness [%]98.698.5
Redundancy11.611.19
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP2772M AMSO4 0.2M NACL, 0.1M CACODYLATE PH 6.5 300 NL SITTING DROPS AT 4 DEGREES

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