274D
CRYSTAL STRUCTURE OF A COVALENT DNA-DRUG ADDUCT: ANTHRAMYCIN BOUND TO C-C-A-A-C-G-T-T-G-G, AND A MOLECULAR EXPLANATION OF SPECIFICITY
Experimental procedure
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS II |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 23.950, 23.950, 88.890 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 2.300 |
R-factor | 0.212 |
RMSD bond length | 0.032 |
RMSD bond angle | 0.061 |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.300 |
Rmerge | 0.064 * |
Number of reflections | 1212 |
Completeness [%] | 90.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | VAPOR DIFFUSION, SITTING DROP, temperature 277.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | METHANOL | ||
3 | 1 | 1 | MPD | ||
4 | 1 | 1 | MGCL2 | ||
5 | 1 | 2 | WATER | ||
6 | 1 | 2 | MPD |