Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

1ZPK

Crystal structure of the complex of mutant HIV-1 protease (A71V, V82T, I84V) with a hydroxyethylamine peptidomimetic inhibitor BOC-PHE-PSI[R-CH(OH)CH2NH]-PHE-GLU-PHE-NH2

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-1
Synchrotron siteESRF
BeamlineID14-1
Temperature [K]100
Detector technologyCCD
Collection date2000-04-12
DetectorMARRESEARCH
Wavelength(s)0.934
Spacegroup nameP 61
Unit cell lengths62.483, 62.483, 82.412
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution10.000 - 1.650
R-factor0.1586
Rwork0.156
R-free0.25280
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1a9m
RMSD bond length0.007
RMSD bond angle0.026
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareAMoRE
Refinement softwareSHELXL-97
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0001.690
High resolution limit [Å]1.6501.650
Rmerge0.0390.370
Number of reflections21955
<I/σ(I)>48.42.3
Completeness [%]99.999.8
Redundancy6.93
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1microseeding4.42980.5 M NaCl, 0.1 M Na Citrate, 10% Glycerol, pH 4.4, microseeding, temperature 298K

217705

PDB entries from 2024-03-27

PDB statisticsPDBj update infoContact PDBjnumon