1ZBH
3'-end specific recognition of histone mRNA stem-loop by 3'-exonuclease
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4A |
Synchrotron site | NSLS |
Beamline | X4A |
Temperature [K] | 100 |
Collection date | 2004-10-20 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 50.386, 195.148, 87.966 |
Unit cell angles | 90.00, 92.13, 90.00 |
Refinement procedure
Resolution | 19.920 - 3.000 |
R-factor | 0.21426 |
Rwork | 0.209 |
R-free | 0.25970 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.094 |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 19.920 |
High resolution limit [Å] | 3.000 |
Number of reflections | 33770 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | pH 6.5 |