1W63
AP1 clathrin adaptor core
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 32 1 2 |
Unit cell lengths | 178.140, 178.140, 1134.994 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.000 - 4.000 |
R-factor | 0.2972 |
Rwork | 0.297 |
R-free | 0.30970 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1GW5 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.861 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.840 | 4.100 |
High resolution limit [Å] | 4.010 | 4.000 |
Rmerge | 0.120 | 0.470 |
Number of reflections | 141015 | |
<I/σ(I)> | 9.4 | 2.5 |
Completeness [%] | 81.3 | 69.7 |
Redundancy | 6.5 | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 8-9% ETHANOL, 0.1 M NA HEPES, PH 7.5, 2 MM CYSTEINE |