1TXD
Crystal Structure of the DH/PH domains of Leukemia-associated RhoGEF
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-BM-D |
Synchrotron site | APS |
Beamline | 14-BM-D |
Temperature [K] | 90 |
Detector technology | CCD |
Collection date | 2002-08-21 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 193.606, 45.859, 74.730 |
Unit cell angles | 90.00, 107.49, 90.00 |
Refinement procedure
Resolution | 24.850 - 2.130 |
R-factor | 0.23676 |
Rwork | 0.235 |
R-free | 0.27433 |
Structure solution method | MIRAS |
RMSD bond length | 0.017 |
RMSD bond angle | 1.486 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | MLPHARE |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.210 |
High resolution limit [Å] | 2.130 | 2.130 |
Number of reflections | 36990 | |
<I/σ(I)> | 21 | 3.3 |
Completeness [%] | 98.3 | 93.7 |
Redundancy | 4 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | PEG3350, sodium chloride, sodium citrate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |