1SCN
INACTIVATION OF SUBTILISIN CARLSBERG BY N-(TERT-BUTOXYCARBONYL-ALANYL-PROLYL-PHENYLALANYL)-O-BENZOL HYDROXYLAMINE: FORMATION OF COVALENT ENZYME-INHIBITOR LINKAGE IN THE FORM OF A CARBAMATE DERIVATIVE
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 76.500, 55.400, 53.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.900 |
R-factor | 0.191 |
RMSD bond length | 0.010 |
RMSD bond angle | 3.200 |
Refinement software | TNT |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.900 * |
Rmerge | 0.115 * |
Total number of observations | 38539 * |
Number of reflections | 17548 * |
Completeness [%] | 87.6 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Batch method * |