1QXL

Crystal structure of Adenosine deaminase complexed with FR235380

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL24XU
Synchrotron site	SPring-8
Beamline	BL24XU
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2003-06-30
Detector	RIGAKU RAXIS
Wavelength(s)	0.836
Spacegroup name	P 43 21 2
Unit cell lengths	78.370, 78.370, 137.820
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	51.250 - 2.250
R-factor	0.24
Rwork	0.232
R-free	0.25300
Structure solution method	MOLECULAR REPLACEMENT
Phasing software	AMoRE
Refinement software	CNX

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	51.250	2.350
High resolution limit [Å]	2.250	2.250
Rmerge	0.090	0.338
Number of reflections	20752
Completeness [%]	98.1	96.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	6	293	Ammonium phosphate, PEG400, MES, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 293K