1QPV
YEAST COFILIN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 290 |
Detector technology | AREA DETECTOR |
Collection date | 1995-02-15 |
Detector | SIEMENS |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 30.780, 46.043, 87.703 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 3.000 |
R-factor | 0.209 |
Rwork | 0.202 |
R-free | 0.28400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1cof |
RMSD bond length | 0.003 |
RMSD bond angle | 0.630 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.200 | 3.100 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.083 | 0.185 |
Number of reflections | 2377 | |
<I/σ(I)> | 19.8 | 4.9 |
Completeness [%] | 89.1 | 77.4 |
Redundancy | 2.9 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 290 | PEG 4000 , pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 290K |