1PGR
2:2 COMPLEX OF G-CSF WITH ITS RECEPTOR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-6B |
Synchrotron site | Photon Factory |
Beamline | BL-6B |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1997-12 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 125.725, 125.725, 373.305 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 3.500 |
Rwork | 0.317 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1igr |
RMSD bond length | 0.012 |
RMSD bond angle | 2.000 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 3.500 |
Rmerge | 0.198 |
Total number of observations | 173168 * |
Number of reflections | 26690 * |
Completeness [%] | 69.1 |
Redundancy | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7.5 | manuscript in preparation * |