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1O5M

Structure of FPT bound to the inhibitor SCH66336

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date1998-04-02
DetectorRIGAKU RAXIS IV
Spacegroup nameP 61
Unit cell lengths171.110, 171.110, 69.310
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution8.000 - 2.300
R-factor0.174
Rwork0.174
Structure solution methodMOLECULAR REPLACEMENT
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareX-PLOR
Refinement softwareX-PLOR
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.380
High resolution limit [Å]2.3002.300
Rmerge0.0550.211

*

Number of reflections49482
<I/σ(I)>23.3
Completeness [%]95.971.9
Redundancy3.53
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP5

*

4

*

Wu, Z., (1999) Protein Eng., 12, 341.

*

Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropethanol23.6 (mM)
21dropDMSO50 (mM)
31reservoir0.1 (M)
41reservoirsodium acetate0.1 (M)pH5.0

217705

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