1HPT
THREE-DIMENSIONAL STRUCTURE OF A RECOMBINANT VARIANT OF HUMAN PANCREATIC SECRETORY TRYPSIN INHIBITOR (KAZAL TYPE)
Experimental procedure
Spacegroup name | P 43 |
Unit cell lengths | 40.150, 40.150, 33.910 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.300 |
R-factor | 0.191 |
Rwork | 0.191 |
RMSD bond length | 0.011 |
RMSD bond angle | 2.700 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 2.460 * |
High resolution limit [Å] | 2.300 * |
Rmerge | 0.069 * |
Total number of observations | 2200 * |
Number of reflections | 4612 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 8.3 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 2 | ammonium sulfate | 2.0 (M) | |
2 | 1 | 2 | Tris-HCl | 100 (mM) | |
3 | 1 | 1 | inhibitor | 10 (mg/ml) |