1HCQ
THE CRYSTAL STRUCTURE OF THE ESTROGEN RECEPTOR DNA-BINDING DOMAIN BOUND TO DNA: HOW RECEPTORS DISCRIMINATE BETWEEN THEIR RESPONSE ELEMENTS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 51.600, 90.800, 114.600 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | ? - 2.400 |
R-factor | 0.204 |
Rwork | 0.204 |
RMSD bond length | 0.018 * |
RMSD bond angle | 2.550 * |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 * | |
High resolution limit [Å] | 2.400 * | 2.400 * |
Rmerge | 0.107 * | 0.402 * |
Total number of observations | 98492 * | |
Number of reflections | 20360 * | |
Completeness [%] | 93.9 * | 87.3 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6 * | 8 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | DNA duplex | 0.07 (mM) | |
10 | 1 | reservoir | methyl pentane | 8 (%) | or ethanol |
2 | 1 | drop | 440-525 | 0.14 (mM) | |
3 | 1 | drop | 1.8 (mM) | ||
4 | 1 | drop | 25 (mM) | ||
5 | 1 | drop | MES | ||
6 | 1 | drop | spermine | 1.8 (mM) | |
7 | 1 | drop | 0.002 (mM) | ||
8 | 1 | reservoir | 0.2 (M) | ||
9 | 1 | reservoir | MES |