1FRB
FR-1 PROTEIN/NADPH/ZOPOLRESTAT COMPLEX
Experimental procedure
Detector technology | AREA DETECTOR |
Collection date | 1995-05-19 |
Detector | XUONG-HAMLIN MULTIWIRE |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 59.450, 65.380, 90.290 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.700 |
R-factor | 0.158 |
Rwork | 0.158 |
RMSD bond length | 0.008 |
Data reduction software | SDMS (DETECTOR SYSTEM (NIELSEN)) |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
High resolution limit [Å] | 1.700 * | 1.700 * |
Rmerge | 0.046 | |
Total number of observations | 213331 * | |
Number of reflections | 43337 | |
Completeness [%] | 94.3 | 90 * |
Redundancy | 4.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 5 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | ALR2 | 7 (mg/ml) | |
2 | 1 | drop | zopolrestat | 0.2 (mM) | |
3 | 1 | drop | 2-mercaptoethanol | 3.5 (mM) | |
4 | 1 | drop | citrate | 25 (mM) | |
5 | 1 | reservoir | PEG6000 | 17 (%) | |
6 | 1 | reservoir | 2-mercaptoethanol | 7 (mM) | |
7 | 1 | reservoir | citrate | 50 (mM) |