1FD0
ISOTYPE SELECTIVITY OF THE HUMAN RETINOIC ACID NUCLEAR RECEPTOR HRAR: THE COMPLEX WITH THE RARGAMMA-SELECTIVE RETINOID SR11254
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | BW7B |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1998-07-11 |
Detector | MARRESEARCH |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 59.789, 59.789, 155.688 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 1.380 |
R-factor | 0.131 |
Rwork | 0.130 |
R-free | 0.15800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1fcy |
RMSD bond length | 0.013 |
RMSD bond angle | 2.387 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.410 |
High resolution limit [Å] | 1.380 | 1.380 |
Rmerge | 0.042 | 0.362 |
Total number of observations | 291021 * | |
Number of reflections | 59004 | |
<I/σ(I)> | 36 | 3.3 |
Completeness [%] | 99.8 | 99.8 |
Redundancy | 4.9 * | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 17 * | sodium acetate, pH 7.0, VAPOR DIFFUSION, HANGING DROP at 290K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PIPES | 0.1 (M) | pH7.0 |
2 | 1 | reservoir | 0.3 (M) | ||
3 | 1 | drop | protein | 3.7 (mg/ml) |