1BTH
STRUCTURE OF THROMBIN COMPLEXED WITH BOVINE PANCREATIC TRYPSIN INHIBITOR
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1995-10-10 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 71.200, 74.500, 83.400 |
Unit cell angles | 90.00, 92.50, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.300 |
R-factor | 0.196 |
Rwork | 0.196 |
R-free | 0.27100 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.690 |
Data reduction software | MOSFLM |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 9999.000 * | |
High resolution limit [Å] | 2.300 * | 2.300 * |
Rmerge | 0.100 | 0.303 * |
Total number of observations | 98344 * | |
Number of reflections | 37833 * | |
Completeness [%] | 1.0 | 97.8 * |
Redundancy | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 20 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | mPEG5000 | 20 (%) | |
2 | 1 | reservoir | HEPES | 0.1 (M) |