1G30
THROMBIN INHIBITOR COMPLEX
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 1997-09-01 |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.54 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 69.300, 70.900, 72.800 |
| Unit cell angles | 90.00, 100.30, 90.00 |
Refinement procedure
| Resolution | 15.980 - 2.000 |
| R-factor | 0.21 * |
| Rwork | 0.210 |
| R-free | 0.26400 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.760 * |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | X-PLOR |
| Refinement software | CNX (2000) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 15.800 |
| High resolution limit [Å] | 2.000 |
| Rmerge | 0.055 |
| Total number of observations | 53146 * |
| Number of reflections | 22489 |
| <I/σ(I)> | 10 |
| Completeness [%] | 94.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | other * | Skrzypczak-Jankun, E., (1991) J. Mol. Biol., 221, 1379. * |
