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- PDB-6qpa: Halothiobacillus neapolitanus sulfur oxygenase reductase -

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基本情報

登録情報
データベース: PDB / ID: 6qpa
タイトルHalothiobacillus neapolitanus sulfur oxygenase reductase
要素Sulfur oxygenase/reductase
キーワードOXIDOREDUCTASE / SULFUR OXYGENASE REDUCTASE / 2-HIS-1-CARBOXYLATE FACIAL TRIAD / CYSTEINE PERSULPHURATION / BIOGEOCHEMICAL SULFUR CYCLE
機能・相同性sulfur oxygenase/reductase / sulfur oxygenase/reductase activity / Sulphur oxygenase reductase / Sulphur oxygenase reductase / Dimeric alpha-beta barrel / : / Sulfur oxygenase/reductase
機能・相同性情報
生物種Halothiobacillus neapolitanus (紅色硫黄細菌)
手法X線回折 / シンクロトロン / 分子置換 / 解像度: 2.1 Å
データ登録者Frazao, C. / Klezin, A. / Poell, U. / Veith, A. / Ruehl, P. / Coelho, R.
資金援助 ポルトガル, ドイツ, 3件
組織認可番号
Foundation for Science and Technology (FCT)LIOA-01-0145-FEDER-007660 ポルトガル
German Research Foundation (DFG)Kl885-6/1 ドイツ
German Research Foundation (DFG)Kl885-7/1 ドイツ
引用
ジャーナル: To Be Published
タイトル: Multiple sulfane modifications in active-site cysteine thiols of two sulfur oxygenase reductases and analysis of substrate/product channels
著者: Frazao, C. / Klezin, A. / Poell, U. / Veith, A. / Ruehl, P. / Coelho, R.
#1: ジャーナル: J.Bacteriol. / : 2012
タイトル: The sulfur oxygenase reductase from the mesophilic bacterium Halothiobacillus neapolitanus is a highly active thermozyme.
著者: Veith, A. / Botelho, H.M. / Kindinger, F. / Gomes, C.M. / Kletzin, A.
履歴
登録2019年2月13日登録サイト: PDBE / 処理サイト: PDBE
改定 1.02020年3月18日Provider: repository / タイプ: Initial release
改定 1.12024年1月24日Group: Data collection / Database references ...Data collection / Database references / Derived calculations / Refinement description
カテゴリ: chem_comp_atom / chem_comp_bond ...chem_comp_atom / chem_comp_bond / database_2 / pdbx_initial_refinement_model / pdbx_struct_conn_angle / struct_conn
Item: _database_2.pdbx_DOI / _database_2.pdbx_database_accession ..._database_2.pdbx_DOI / _database_2.pdbx_database_accession / _pdbx_struct_conn_angle.ptnr1_auth_seq_id / _pdbx_struct_conn_angle.ptnr3_auth_seq_id / _pdbx_struct_conn_angle.value / _struct_conn.conn_type_id / _struct_conn.id / _struct_conn.pdbx_dist_value / _struct_conn.pdbx_leaving_atom_flag / _struct_conn.ptnr1_auth_asym_id / _struct_conn.ptnr1_auth_comp_id / _struct_conn.ptnr1_auth_seq_id / _struct_conn.ptnr1_label_asym_id / _struct_conn.ptnr1_label_atom_id / _struct_conn.ptnr1_label_comp_id / _struct_conn.ptnr1_label_seq_id / _struct_conn.ptnr2_auth_asym_id / _struct_conn.ptnr2_auth_comp_id / _struct_conn.ptnr2_auth_seq_id / _struct_conn.ptnr2_label_asym_id / _struct_conn.ptnr2_label_atom_id / _struct_conn.ptnr2_label_comp_id / _struct_conn.ptnr2_label_seq_id

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構造の表示

構造ビューア分子:
MolmilJmol/JSmol

ダウンロードとリンク

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集合体

登録構造単位
A: Sulfur oxygenase/reductase
B: Sulfur oxygenase/reductase
C: Sulfur oxygenase/reductase
D: Sulfur oxygenase/reductase
E: Sulfur oxygenase/reductase
F: Sulfur oxygenase/reductase
G: Sulfur oxygenase/reductase
H: Sulfur oxygenase/reductase
I: Sulfur oxygenase/reductase
J: Sulfur oxygenase/reductase
K: Sulfur oxygenase/reductase
L: Sulfur oxygenase/reductase
M: Sulfur oxygenase/reductase
N: Sulfur oxygenase/reductase
O: Sulfur oxygenase/reductase
P: Sulfur oxygenase/reductase
Q: Sulfur oxygenase/reductase
R: Sulfur oxygenase/reductase
T: Sulfur oxygenase/reductase
U: Sulfur oxygenase/reductase
V: Sulfur oxygenase/reductase
W: Sulfur oxygenase/reductase
Y: Sulfur oxygenase/reductase
Z: Sulfur oxygenase/reductase
ヘテロ分子


分子量 (理論値)分子数
合計 (水以外)855,66196
ポリマ-849,70924
非ポリマー5,95172
71,2493955
1


  • 登録構造と同一
  • 登録者・ソフトウェアが定義した集合体
  • 根拠: microscopy
タイプ名称対称操作
identity operation1_555x,y,z1
Buried area144820 Å2
ΔGint-1724 kcal/mol
Surface area223550 Å2
手法PISA
単位格子
Length a, b, c (Å)200.840, 212.450, 215.980
Angle α, β, γ (deg.)90.000, 90.000, 90.000
Int Tables number19
Space group name H-MP212121
非結晶学的対称性 (NCS)NCSドメイン:
IDEns-ID詳細
11(chain A and (resid 6 through 210 or resid 212...
21(chain B and (resid 6 through 210 or resid 212...
31(chain C and (resid 6 through 210 or resid 212...
41(chain D and (resid 6 through 210 or resid 212...
51(chain E and (resid 6 through 210 or resid 212...
61(chain F and (resid 6 through 210 or resid 212...
71(chain G and (resid 6 through 210 or resid 212...
81(chain H and (resid 6 through 210 or resid 212...
91(chain I and (resid 6 through 210 or resid 212...
101(chain J and (resid 6 through 210 or resid 212...
111(chain K and (resid 6 through 210 or resid 212...
121(chain L and (resid 6 through 210 or resid 212...
131(chain M and (resid 6 through 210 or resid 212...
141(chain N and (resid 6 through 210 or resid 212...
151(chain O and (resid 6 through 210 or resid 212...
161(chain P and (resid 6 through 210 or resid 212...
171(chain Q and (resid 6 through 210 or resid 212...
181(chain R and (resid 6 through 210 or resid 212...
191(chain T and (resid 6 through 210 or resid 212...
201(chain U and (resid 6 through 210 or resid 212...
211(chain V and (resid 6 through 210 or resid 212...
221(chain W and (resid 6 through 210 or resid 212...
231(chain Y and (resid 6 through 210 or resid 212...
241(chain Z and (resid 6 through 210 or resid 212...

NCSドメイン領域:
Dom-IDComponent-IDEns-IDSelection detailsAuth asym-IDAuth seq-ID
111(chain A and (resid 6 through 210 or resid 212...A6 - 210
121(chain A and (resid 6 through 210 or resid 212...A212 - 301
131(chain A and (resid 6 through 210 or resid 212...A303 - 312
141(chain A and (resid 6 through 210 or resid 212...A315 - 317
151(chain A and (resid 6 through 210 or resid 212...A319
211(chain B and (resid 6 through 210 or resid 212...B6 - 210
221(chain B and (resid 6 through 210 or resid 212...B212 - 301
231(chain B and (resid 6 through 210 or resid 212...B303 - 312
241(chain B and (resid 6 through 210 or resid 212...B315 - 317
251(chain B and (resid 6 through 210 or resid 212...B319
311(chain C and (resid 6 through 210 or resid 212...C6 - 210
321(chain C and (resid 6 through 210 or resid 212...C212 - 301
331(chain C and (resid 6 through 210 or resid 212...C303 - 312
341(chain C and (resid 6 through 210 or resid 212...C315 - 317
351(chain C and (resid 6 through 210 or resid 212...C320
411(chain D and (resid 6 through 210 or resid 212...D6 - 210
421(chain D and (resid 6 through 210 or resid 212...D212 - 301
431(chain D and (resid 6 through 210 or resid 212...D303 - 312
441(chain D and (resid 6 through 210 or resid 212...D315 - 318
451(chain D and (resid 6 through 210 or resid 212...D320
511(chain E and (resid 6 through 210 or resid 212...E6 - 210
521(chain E and (resid 6 through 210 or resid 212...E212 - 301
531(chain E and (resid 6 through 210 or resid 212...E303 - 312
541(chain E and (resid 6 through 210 or resid 212...E315 - 317
551(chain E and (resid 6 through 210 or resid 212...E320
611(chain F and (resid 6 through 210 or resid 212...F6 - 210
621(chain F and (resid 6 through 210 or resid 212...F212 - 301
631(chain F and (resid 6 through 210 or resid 212...F303 - 312
641(chain F and (resid 6 through 210 or resid 212...F315 - 317
651(chain F and (resid 6 through 210 or resid 212...F319
711(chain G and (resid 6 through 210 or resid 212...G6 - 210
721(chain G and (resid 6 through 210 or resid 212...G212 - 301
731(chain G and (resid 6 through 210 or resid 212...G303 - 312
741(chain G and (resid 6 through 210 or resid 212...G315 - 317
751(chain G and (resid 6 through 210 or resid 212...G319
811(chain H and (resid 6 through 210 or resid 212...H6 - 210
821(chain H and (resid 6 through 210 or resid 212...H212 - 301
831(chain H and (resid 6 through 210 or resid 212...H303 - 312
841(chain H and (resid 6 through 210 or resid 212...H315 - 317
851(chain H and (resid 6 through 210 or resid 212...H320
911(chain I and (resid 6 through 210 or resid 212...I6 - 210
921(chain I and (resid 6 through 210 or resid 212...I212 - 301
931(chain I and (resid 6 through 210 or resid 212...I303 - 312
941(chain I and (resid 6 through 210 or resid 212...I315 - 317
951(chain I and (resid 6 through 210 or resid 212...I319
1011(chain J and (resid 6 through 210 or resid 212...J6 - 210
1021(chain J and (resid 6 through 210 or resid 212...J212 - 301
1031(chain J and (resid 6 through 210 or resid 212...J303 - 312
1041(chain J and (resid 6 through 210 or resid 212...J315 - 317
1051(chain J and (resid 6 through 210 or resid 212...J319
1111(chain K and (resid 6 through 210 or resid 212...K6 - 210
1121(chain K and (resid 6 through 210 or resid 212...K212 - 301
1131(chain K and (resid 6 through 210 or resid 212...K303 - 312
1141(chain K and (resid 6 through 210 or resid 212...K315 - 317
1151(chain K and (resid 6 through 210 or resid 212...K319
1211(chain L and (resid 6 through 210 or resid 212...L6 - 210
1221(chain L and (resid 6 through 210 or resid 212...L212 - 301
1231(chain L and (resid 6 through 210 or resid 212...L303 - 312
1241(chain L and (resid 6 through 210 or resid 212...L315 - 317
1251(chain L and (resid 6 through 210 or resid 212...L320
1311(chain M and (resid 6 through 210 or resid 212...M6 - 210
1321(chain M and (resid 6 through 210 or resid 212...M212 - 301
1331(chain M and (resid 6 through 210 or resid 212...M303 - 312
1341(chain M and (resid 6 through 210 or resid 212...M315 - 317
1351(chain M and (resid 6 through 210 or resid 212...M319
1411(chain N and (resid 6 through 210 or resid 212...N6 - 210
1421(chain N and (resid 6 through 210 or resid 212...N212 - 301
1431(chain N and (resid 6 through 210 or resid 212...N303 - 312
1441(chain N and (resid 6 through 210 or resid 212...N315 - 317
1451(chain N and (resid 6 through 210 or resid 212...N319
1511(chain O and (resid 6 through 210 or resid 212...O6 - 210
1521(chain O and (resid 6 through 210 or resid 212...O212 - 301
1531(chain O and (resid 6 through 210 or resid 212...O303 - 312
1541(chain O and (resid 6 through 210 or resid 212...O315 - 317
1551(chain O and (resid 6 through 210 or resid 212...O319
1611(chain P and (resid 6 through 210 or resid 212...P6 - 210
1621(chain P and (resid 6 through 210 or resid 212...P212 - 301
1631(chain P and (resid 6 through 210 or resid 212...P303 - 312
1641(chain P and (resid 6 through 210 or resid 212...P315 - 317
1651(chain P and (resid 6 through 210 or resid 212...P319
1711(chain Q and (resid 6 through 210 or resid 212...Q6 - 210
1721(chain Q and (resid 6 through 210 or resid 212...Q212 - 301
1731(chain Q and (resid 6 through 210 or resid 212...Q303 - 312
1741(chain Q and (resid 6 through 210 or resid 212...Q315 - 317
1751(chain Q and (resid 6 through 210 or resid 212...Q319
1811(chain R and (resid 6 through 210 or resid 212...R6 - 210
1821(chain R and (resid 6 through 210 or resid 212...R212 - 301
1831(chain R and (resid 6 through 210 or resid 212...R303 - 312
1841(chain R and (resid 6 through 210 or resid 212...R315 - 317
1851(chain R and (resid 6 through 210 or resid 212...R319
1911(chain T and (resid 6 through 210 or resid 212...T6 - 210
1921(chain T and (resid 6 through 210 or resid 212...T212 - 301
1931(chain T and (resid 6 through 210 or resid 212...T303 - 312
1941(chain T and (resid 6 through 210 or resid 212...T315 - 318
1951(chain T and (resid 6 through 210 or resid 212...T320
2011(chain U and (resid 6 through 210 or resid 212...U6 - 210
2021(chain U and (resid 6 through 210 or resid 212...U212 - 301
2031(chain U and (resid 6 through 210 or resid 212...U303 - 312
2041(chain U and (resid 6 through 210 or resid 212...U315 - 317
2051(chain U and (resid 6 through 210 or resid 212...U319
2111(chain V and (resid 6 through 210 or resid 212...V6 - 210
2121(chain V and (resid 6 through 210 or resid 212...V212 - 301
2131(chain V and (resid 6 through 210 or resid 212...V303 - 312
2141(chain V and (resid 6 through 210 or resid 212...V315 - 318
2151(chain V and (resid 6 through 210 or resid 212...V320
2211(chain W and (resid 6 through 210 or resid 212...W6 - 210
2221(chain W and (resid 6 through 210 or resid 212...W212 - 301
2231(chain W and (resid 6 through 210 or resid 212...W303 - 312
2241(chain W and (resid 6 through 210 or resid 212...W315 - 317
2251(chain W and (resid 6 through 210 or resid 212...W319
2311(chain Y and (resid 6 through 210 or resid 212...Y6 - 210
2321(chain Y and (resid 6 through 210 or resid 212...Y212 - 301
2331(chain Y and (resid 6 through 210 or resid 212...Y303 - 312
2341(chain Y and (resid 6 through 210 or resid 212...Y315 - 318
2351(chain Y and (resid 6 through 210 or resid 212...Y320
2411(chain Z and (resid 6 through 210 or resid 212...Z6 - 210
2421(chain Z and (resid 6 through 210 or resid 212...Z212 - 301
2431(chain Z and (resid 6 through 210 or resid 212...Z303 - 312
2441(chain Z and (resid 6 through 210 or resid 212...Z315 - 317
2451(chain Z and (resid 6 through 210 or resid 212...Z319

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要素

#1: タンパク質 ...
Sulfur oxygenase/reductase


分子量: 35404.555 Da / 分子数: 24 / 変異: CSS_33, CSS_103 / 由来タイプ: 組換発現
由来: (組換発現) Halothiobacillus neapolitanus (strain ATCC 23641 / c2) (紅色硫黄細菌)
遺伝子: Hneap_1222 / 発現宿主: Escherichia coli (大腸菌) / 参照: UniProt: D0L035, sulfur oxygenase/reductase
#2: 化合物...
ChemComp-FE / FE (III) ION


分子量: 55.845 Da / 分子数: 24 / 由来タイプ: 合成 / : Fe / タイプ: SUBJECT OF INVESTIGATION
#3: 化合物...
ChemComp-SO4 / SULFATE ION / 硫酸ジアニオン


分子量: 96.063 Da / 分子数: 48 / 由来タイプ: 合成 / : SO4 / タイプ: SUBJECT OF INVESTIGATION
#4: 水 ChemComp-HOH / water


分子量: 18.015 Da / 分子数: 3955 / 由来タイプ: 天然 / : H2O
研究の焦点であるリガンドがあるかY

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実験情報

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実験

実験手法: X線回折 / 使用した結晶の数: 1

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試料調製

結晶マシュー密度: 2.63 Å3/Da / 溶媒含有率: 53.16 %
結晶化温度: 298 K / 手法: 蒸気拡散法, シッティングドロップ法 / pH: 6.4 / 詳細: 0.1 M ADA pH 6.4, 1 M ammomium sulfate

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データ収集

回折平均測定温度: 100 K / Serial crystal experiment: N
放射光源由来: シンクロトロン / サイト: ESRF / ビームライン: ID29 / 波長: 0.96112 Å
検出器タイプ: DECTRIS PILATUS 6M / 検出器: PIXEL / 日付: 2013年6月20日
放射プロトコル: SINGLE WAVELENGTH / 単色(M)・ラウエ(L): M / 散乱光タイプ: x-ray
放射波長波長: 0.96112 Å / 相対比: 1
反射解像度: 2.1→83.695 Å / Num. obs: 532671 / % possible obs: 100 % / 冗長度: 13.534 % / Biso Wilson estimate: 36.88 Å2 / CC1/2: 0.999 / Rmerge(I) obs: 0.153 / Rrim(I) all: 0.159 / Χ2: 0.998 / Net I/σ(I): 14.78 / Num. measured all: 7209077 / Scaling rejects: 854
反射 シェル

Diffraction-ID: 1

解像度 (Å)冗長度 (%)Rmerge(I) obsMean I/σ(I) obsNum. unique obsCC1/2Rrim(I) all% possible all
2.1-2.1711.7170.151.29495180.490.159100
2.17-2.2412.3421.7211.65435400.6221.796100
2.24-2.3114.1331.3952.21384980.751.446100
2.31-2.3914.2271.042.94386510.8451.078100
2.39-2.4814.0910.8053.76377640.90.835100
2.48-2.5813.8350.6344.72359830.9330.658100
2.58-2.713.1270.5015.76364620.9490.522100
2.7-2.8313.7030.3578.1329340.9740.371100
2.83-2.9814.280.27310.62311780.9860.283100
2.98-3.1614.1520.19514.39300390.9930.202100
3.16-3.3813.8930.13320.16286310.9960.138100
3.38-3.6512.9780.09725.82263980.9980.101100
3.65-414.4740.07635244710.9990.079100
4-4.4714.160.05645.03219940.9990.058100
4.47-5.1613.1990.0548.07195610.9990.052100
5.16-6.3213.8330.05344.61166500.9990.055100
6.32-8.9413.7150.04352.2130220.9990.045100
8.94-83.69512.7720.0370.1373770.9990.03299.5

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解析

ソフトウェア
名称バージョン分類
PHENIX1.13_2998精密化
XDSデータ削減
XSCALEデータスケーリング
PHASER位相決定
精密化構造決定の手法: 分子置換
開始モデル: 2cb2
解像度: 2.1→83.695 Å / SU ML: 0.25 / 交差検証法: THROUGHOUT / σ(F): 1.43 / 位相誤差: 21.57
Rfactor反射数%反射Selection details
Rfree0.2004 1998 0.38 %thin spherical resolution bins
Rwork0.1622 ---
obs0.1623 532671 99.9 %-
溶媒の処理減衰半径: 0.9 Å / VDWプローブ半径: 1.11 Å
原子変位パラメータBiso max: 142.04 Å2 / Biso mean: 45.7773 Å2 / Biso min: 16.2 Å2
精密化ステップサイクル: final / 解像度: 2.1→83.695 Å
タンパク質核酸リガンド溶媒全体
原子数58671 0 264 3955 62890
Biso mean--108.54 48.34 -
残基数----7439
Refine LS restraints NCS
Ens-IDDom-IDAuth asym-IDRefine-IDRmsタイプ
11A35820X-RAY DIFFRACTION7.278TORSIONAL
12B35820X-RAY DIFFRACTION7.278TORSIONAL
13C35820X-RAY DIFFRACTION7.278TORSIONAL
14D35820X-RAY DIFFRACTION7.278TORSIONAL
15E35820X-RAY DIFFRACTION7.278TORSIONAL
16F35820X-RAY DIFFRACTION7.278TORSIONAL
17G35820X-RAY DIFFRACTION7.278TORSIONAL
18H35820X-RAY DIFFRACTION7.278TORSIONAL
19I35820X-RAY DIFFRACTION7.278TORSIONAL
110J35820X-RAY DIFFRACTION7.278TORSIONAL
111K35820X-RAY DIFFRACTION7.278TORSIONAL
112L35820X-RAY DIFFRACTION7.278TORSIONAL
113M35820X-RAY DIFFRACTION7.278TORSIONAL
114N35820X-RAY DIFFRACTION7.278TORSIONAL
115O35820X-RAY DIFFRACTION7.278TORSIONAL
116P35820X-RAY DIFFRACTION7.278TORSIONAL
117Q35820X-RAY DIFFRACTION7.278TORSIONAL
118R35820X-RAY DIFFRACTION7.278TORSIONAL
119T35820X-RAY DIFFRACTION7.278TORSIONAL
120U35820X-RAY DIFFRACTION7.278TORSIONAL
121V35820X-RAY DIFFRACTION7.278TORSIONAL
122W35820X-RAY DIFFRACTION7.278TORSIONAL
123Y35820X-RAY DIFFRACTION7.278TORSIONAL
124Z35820X-RAY DIFFRACTION7.278TORSIONAL
LS精密化 シェル

Refine-ID: X-RAY DIFFRACTION / Rfactor Rfree error: 0

解像度 (Å)Rfactor RfreeNum. reflection RfreeRfactor RworkNum. reflection Rwork% reflection obs (%)
2.1-2.15210.34291490.28883722099
2.1521-2.21030.36041490.266937693100
2.2103-2.27530.28131340.247637636100
2.2753-2.34880.26481470.219637742100
2.3488-2.43270.261310.203737710100
2.4327-2.53010.25231480.186537744100
2.5301-2.64530.22151340.185237779100
2.6453-2.78480.21891400.178737845100
2.7848-2.95930.26181570.173737865100
2.9593-3.18780.20161310.165737912100
3.1878-3.50860.1871590.156937912100
3.5086-4.01620.16981140.134938167100
4.0162-5.060.15291760.115338229100
5.06-83.6590.15041290.147139016100
精密化 TLS

手法: refined / Refine-ID: X-RAY DIFFRACTION

IDL112)L122)L132)L222)L232)L332)S11 (Å °)S12 (Å °)S13 (Å °)S21 (Å °)S22 (Å °)S23 (Å °)S31 (Å °)S32 (Å °)S33 (Å °)T112)T122)T132)T222)T232)T332)Origin x (Å)Origin y (Å)Origin z (Å)
10.24240.08170.21580.3741-0.10780.21330.0745-0.1701-0.19260.28060.16450.16840.38870.46240.01570.40480.10420.0020.3145-0.04450.2888-19.8063137.705144.0763
20.0673-0.04110.01950.0391-0.04340.03410.00540.1420.10060.0295-0.05320.08540.1906-0.0430.00010.42390.0279-0.00690.3539-0.03140.4036-15.0813138.7032153.929
30.08690.12490.00370.1694-0.08470.2030.0090.0383-0.1079-0.21180.02970.06410.09360.04120.00010.35070.0448-0.05920.2851-0.04310.3518-28.6985129.8945133.6629
40.0138-0.00520.00980.0398-0.00230.0328-0.1373-0.1983-0.2874-0.1707-0.1037-0.0895-0.03040.09250.00010.40830.0009-0.00650.3073-0.03380.3717-23.3029140.0506150.1677
50.07970.0391-0.04180.0621-0.0220.0558-0.1869-0.06980.05150.1590.0362-0.11970.11220.139-0.00010.4148-0.02710.02960.4036-0.07280.4043-14.6989149.5314153.2857
60.1229-0.06440.00740.1960.25660.3702-0.0612-0.1271-0.06280.0265-0.03140.1359-0.01040.00590.00010.36250.02180.01960.2911-0.04560.3281-26.5253141.3398147.4275
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340.1181-0.1294-0.02430.2003-0.05210.0786-0.0681-0.06810.21720.17450.07660.1615-0.1731-0.16500.54330.1849-0.09350.6061-0.0730.314-20.460698.91766.4381
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930.098-0.0806-0.11250.03270.07050.0545-0.0197-0.0061-0.00790.286-0.04430.0155-0.0042-0.0829-0.00010.258-0.0294-0.02020.3168-0.0470.4573-28.601251.4188125.1548
940.16940.08990.07340.05110.09280.2935-0.11940.04580.0128-0.27060.2022-0.0407-0.0106-0.08880.00010.2255-0.0203-0.05180.3318-0.02320.3792-23.068954.2929113.5897
950.1318-0.1020.17240.0378-0.01430.11980.1004-0.11520.05390.1557-0.1440.2090.2362-0.2094-00.3098-0.01580.01230.2681-0.00910.36373.106743.5747126.9248
960.3001-0.0180.17220.22060.00680.5685-0.00080.0897-0.1295-0.0245-0.0180.02230.08570.0497-00.26080.0052-0.0220.2769-0.06280.3772-9.583644.895110.0203
970.0249-0.01380.01930.04460.09420.1210.01470.02550.0648-0.1002-0.0690.1436-0.0961-0.14730.00010.2984-0.0095-0.07060.3544-0.08110.4728-40.218759.6443119.7496
980.1495-0.15760.20420.37990.13230.42620.05440.0695-0.1492-0.0891-0.0565-0.03070.00260.098800.18960.0065-0.03170.2844-0.08060.3128-11.215447.1587105.2083
990.07060.0042-0.11480.06570.03810.1448-0.1049-0.3608-0.19620.4974-0.01470.0798-0.1909-0.03030.00030.29180.0052-0.02580.3834-0.02240.363-9.716648.7408123.7995
1000.08740.02810.0570.02090.03010.1486-0.0649-0.27630.0076-0.11480.14820.02380.00410.0506-0.00020.3350.08420.02360.3632-0.07860.362720.32655.443393.6584
1010.18890.063-0.09070.0337-0.0250.048-0.2145-0.1140.1189-0.28790.26370.27980.6306-0.59540.00150.6086-0.08620.03410.8999-0.11650.97546.776268.357594.8582
1020.0053-0.0132-0.01520.0098-0.00280.01550.15090.0750.16560.1640.2639-0.0714-0.28860.0914-0.00080.52110.03060.04090.5522-0.15270.51597.191250.151990.771
1030.36450.0394-0.19470.3005-0.28210.3206-0.03840.0283-0.0384-0.12060.0099-0.0142-0.0578-0.017200.26050.0350.02170.3669-0.09740.365921.166560.647998.0633
1040.0047-0.0295-0.01020.0416-0.00770.0565-0.25860.378-0.22650.38080.21630.1809-0.0915-0.1927-0.00010.37320.0343-0.07550.507-0.07470.40068.663753.747881.7459
1050.22290.16980.0520.10220.00530.1379-0.04690.0473-0.0973-0.22350.0158-0.22070.13810.044400.26920.02110.0480.3172-0.0850.323122.195656.007892.2427
1060.05160.0236-0.02710.0066-0.02720.02010.03680.018-0.3181-0.1712-0.1535-0.21740.15070.0457-0.00040.25190.04720.00380.321-0.03680.430913.53443.3311118.0753
1070.21430.09030.0930.32440.25820.2459-0.00470.1208-0.1504-0.059-0.0124-0.04820.1234-0.0426-00.21140.06220.01890.2938-0.08030.315729.338952.1759102.6048
1080.0956-0.03080.00520.03010.01820.00950.39480.4314-0.0160.0298-0.20390.1085-0.0187-0.08110.00030.4370.0839-0.02460.5397-0.10730.357412.263559.709572.3226
1090.4384-0.0558-0.17650.446-0.23910.33610.0584-0.0134-0.0089-0.0036-0.0161-0.16290.0160.03480.00770.19060.04810.03820.2815-0.10980.319432.354956.4275100.4002
1100.22420.0113-0.42420.0027-0.02750.90810.11980.5201-0.304-0.2456-0.06690.62890.003-0.53920.10870.2010.00850.04010.3268-0.07910.43515.720948.858103.2163
1110.02080.0466-0.02790.1577-0.13190.0890.13790.1127-0.03410.14490.20280.1682-0.091-0.03420.00110.3022-0.0043-0.11310.3897-0.07420.4075-25.493760.354489.1239
112-0.0130.0422-0.01670.0202-0.00350.00850.38260.1330.17760.3199-0.25120.041-0.41310.0851-0.00060.84230.0353-0.08850.7239-0.0570.6149-14.502570.331884.763
1130.5171-0.36280.21290.3639-0.15550.1762-0.0067-0.0271-0.11590.002-0.04430.0778-0.1044-0.32640.00010.268-0.0391-0.03690.302-0.06660.3164-27.498267.522195.3492
1140.0227-0.0165-0.01050.02170.01880.0084-0.09570.46350.03320.01760.1645-0.01350.05540.60560.01190.377-0.0027-0.06830.3761-0.06130.3359-20.727768.232296.457
1150.0491-0.038-0.02950.0269-0.02260.1497-0.23870.2030.2184-0.3814-0.00130.07150.09490.1042-0.0070.36810.0425-0.0660.4578-0.14130.3541-18.183155.383478.8652
1160.1222-0.0206-0.14050.1687-0.15860.36560.07750.1408-0.133-0.0487-0.08640.10320.16050.0437-0.04550.27540.0313-0.1040.3663-0.13150.3558-23.440557.792791.1297
1170.16410.2216-0.16810.3444-0.26620.2015-0.1840.1894-0.2263-0.57080.1826-0.11510.1833-0.3517-0.04540.38770.0267-0.16060.4769-0.13260.4017-44.790975.808378.5994
1180.0777-0.19090.11050.36120.01030.847-0.0190.0683-0.0929-0.0547-0.05440.10430.0479-0.0543-0.04440.2196-0.0229-0.09120.3032-0.10980.3831-37.764660.99993.8591
1190.79131.1092-0.23932.5306-1.25110.9787-0.04090.0922-0.3235-0.2117-0.4029-0.7191-0.16330.3531-0.16440.35920.0768-0.01480.493-0.14160.4219-4.722550.502884.7844
1200.3950.17940.35890.3898-0.05730.4730.0145-0.0154-0.068-0.0383-0.01230.1009-0.0215-0.069800.2155-0.0061-0.07780.2505-0.09680.3351-35.205959.343498.6436
1210.1384-0.17680.1290.3053-0.24910.20440.02780.4417-0.0301-0.2085-0.3444-0.1906-0.1893-0.0738-0.04190.49250.0253-0.10970.5419-0.08910.4013-32.808267.308382.045
1220.07650.05570.04870.172-0.03670.0584-0.21240.1577-0.0152-0.150.0563-0.0305-0.00040.19260.00030.50230.0980.0150.5946-0.09050.26523.728481.909458.1261
1230.0131-0.0914-0.01850.08450.0255-0.0129-0.2614-0.1750.00540.12690.0858-0.1289-0.25220.1827-0.00190.6810.1349-0.06530.7845-0.09170.54715.784778.251674.5016
1240.42250.29020.14510.21060.01750.06450.07040.05790.1325-0.38660.0511-0.138-0.0396-0.02780.00010.52250.1153-0.03310.4734-0.01970.25563.711191.664964.555
1250.21560.0899-0.10080.044-0.03780.0679-0.1949-0.0777-0.18310.0551-0.0457-0.00750.0567-0.1092-0.02590.49970.1342-0.04550.4776-0.07630.26791.182887.439568.2478
1260.0890.0008-0.04430.169-0.05430.0340.0874-0.045-0.3193-0.2164-0.040.26240.11570.18430.02330.55230.0860.00370.5623-0.12110.35372.944468.385161.2707
1270.00030.0082-0.02470.0249-0.03710.0305-0.1819-0.0326-0.3056-0.32940.01740.01-0.1348-0.3068-0.00060.49720.1123-0.02120.528-0.12420.4215-4.993680.041667.2015
1280.3031-0.28210.24630.87520.00660.23270.0240.44760.1521-0.2347-0.0206-0.2460.02480.2714-0.05230.55780.09990.04980.5081-0.05350.161916.7388.434556.2042
1290.59720.10660.19190.1241-0.01270.31780.2830.3858-0.7294-0.4033-0.088-0.11330.09590.09910.54570.65030.24110.12630.6445-0.1034-0.497810.196292.454752.5964
1300.0384-0.00630.05730.0123-0.03440.05650.0199-0.2482-0.0622-0.0740.1324-0.05290.1013-0.41390.00010.44330.0623-0.0630.492-0.07150.3127-10.100664.486567.3585
1310.7139-0.0806-0.28670.14210.05280.34550.05180.17660.0657-0.1916-0.0395-0.0564-0.1155-0.043-0.00060.57430.1236-0.04480.5164-0.04420.21731.009194.220353.563
132-0.0091-0.019-0.00550.0192-0.01860.0094-0.0047-0.2537-0.3519-0.10680.0033-0.01290.43740.3065-0.00190.37810.10.01530.5166-0.03120.252115.366584.098259.1821
1330.23090.02470.17920.05080.04690.1349-0.2924-0.00410.0696-0.1438-0.1070.23620.1753-0.13290.00010.39440.01740.02850.3766-0.03310.33741.848110.3333166.5304
134-0.01720.04-0.03520.2266-0.21580.2097-0.179-0.0019-0.0512-0.59510.09840.4782-0.3374-0.01790.00420.745-0.0786-0.08250.5657-0.04040.65492.091998.6245158.6779
1350.58970.0778-0.13690.0843-0.10870.1143-0.0365-0.02160.0773-0.06690.0520.00210.1784-0.006900.3556-0.01-0.03590.2621-0.07420.2919-2.6547114.9666160.4258
1360.4216-0.2114-0.04020.10140.02740.0079-0.17750.0508-0.3838-0.1594-0.1178-0.13210.2242-0.041-0.21820.4029-0.0458-0.00840.3329-0.03680.17912.2612112.2948156.4298
1370.1866-0.0649-0.03990.0239-0.0049-0.01070.00820.0022-0.29530.2891-0.1446-0.08680.3425-0.20940.00020.43290.065-0.0180.3583-0.00560.29817.041499.7517173.8131
1380.16290.1255-0.02830.2603-0.15990.08440.08420.0284-0.03840.0282-0.1002-0.0678-0.1016-0.0877-00.3250.0209-0.00190.344-0.02990.23486.8525111.1078167.1956
1390.0160.05370.02740.09210.0620.00710.0009-0.16250.03230.153-0.02420.22240.02270.0610.00010.40380.00650.06140.342-0.04140.291-24.0889108.8936170.3456
1400.26370.20260.20560.20060.06550.33410.0202-0.09480.01220.11670.03420.06640.0079-0.01810.00010.3245-0.00030.02990.2779-0.06870.2008-6.8075120.6662170.5379
141-0.00020.03730.03410.07880.11270.0649-0.0753-0.0332-0.19620.20260.3554-0.37970.10170.35050.00060.39430.0242-0.03020.3959-0.0530.404821.686199.05168.8539
1420.40370.2662-0.19530.45070.0080.52340.0589-0.07580.09070.020.00590.06360.0053-0.0010.00010.3039-0.0019-0.00570.2672-0.0690.2191-2.557123.6298168.2622
1430.13320.06830.04750.06090.03420.0238-0.11870.2541-0.39280.07790.1853-0.0870.5364-0.15570.01550.3661-0.03590.0170.2663-0.03560.2489-10.4038107.1024169.8174
1440.41410.0071-0.01140.1280.14890.1535-0.18730.2210.05630.0406-0.0173-0.65240.0184-0.0032-0.00240.29520.04180.00650.33570.09760.34622.996872.2766150.0443
1450.1596-0.10780.15150.1754-0.16220.1641-0.08530.611-0.1017-0.3071-0.03180.4326-0.025-0.16780.00830.56840.0471-0.07250.58950.03730.504713.90574.4318152.6234
1460.4865-0.0998-0.33860.67090.4260.4373-0.02010.1156-0.04150.0144-0.0207-0.08180.04410.1072-00.26820.00510.00340.29190.03870.2446-0.072568.1824148.5124
147-0.0039-0.006-0.00680.07180.01660.01670.0924-0.0389-0.0475-0.46660.0012-0.32230.1357-0.0334-0.00030.44310.0131-0.06680.404-0.00560.408211.004976.859163.0299
1480.04540.0340.01880.04990.03610.02-0.1728-0.27270.33870.16540.26230.0420.096-0.0932-0.00010.34090.0693-0.02970.3271-0.02260.3253-1.189877.3684155.2743
1490.194-0.02250.05360.0574-0.00710.011-0.08940.0549-0.15610.13620.0973-0.14630.2390.0911-0.00010.3220.0366-0.00870.30620.02630.27716.116355.3866146.4046
150-0.0020.0064-0.00650.0130.05820.248-0.1359-0.3887-0.77640.19260.0103-0.04910.09850.42210.00490.30050.05520.00010.370.10410.425815.215844.2541136.9218
1510.4904-0.08180.1780.03680.06240.38820.0226-0.0137-0.13940.12060.0236-0.02310.12290.043100.24220.00860.02280.20640.03320.2489-4.790456.8765148.54
1520.06430.08150.06540.08930.08330.08010.2766-0.15540.3640.1031-0.07870.2028-0.02060.14010.0020.41770.03330.0030.3529-0.01360.38494.345683.9944169.1347
1530.3798-0.2115-0.03080.5065-0.10350.1625-0.02640.0369-0.07990.07740.05150.08540.02440.062900.21920.01570.00940.22220.03640.1955-8.998759.5872148.7468
1540.15470.0480.13730.04440.02610.0709-0.00680.06950.11350.220.0467-0.6649-0.07760.04380.00010.31580.05960.00080.369-0.00830.33779.530359.8156147.5992
1550.43750.17720.43040.10930.24460.54030.5301-0.2010.2243-0.0299-0.2801-0.15190.3095-0.36610.01030.29930.0859-0.03580.3686-0.07580.372938.348592.024148.7176
1560.1132-0.09080.05230.0360.04190.24820.28810.44920.2374-0.2476-0.306-0.2772-0.1258-0.1050.00250.7480.1065-0.02350.6866-0.15240.640925.327297.6923151.0018
1570.09940.14140.03090.35770.05540.10440.004-0.0195-0.0011-0.04380.1387-0.2159-0.056-0.06820.00020.3080.0680.00780.3317-0.06290.379639.548195.5893141.3472
1580.05130.04120.09030.06030.0860.30230.0731-0.23470.54080.0627-0.2639-0.18520.2584-0.3067-0.01350.34740.0914-0.02230.3884-0.07470.460532.816893.7798139.6542
1590.20950.0528-0.18480.07540.01140.1187-0.3143-0.15330.03740.29810.2130.01460.047-0.0032-00.38840.0402-0.06890.4232-0.05950.3834.130590.1389162.101
1600.0748-0.0096-0.10660.00030.01720.12380.17680.2273-0.03930.0786-0.0309-0.12480.13530.12500.34070.015-0.03570.3617-0.06640.329637.407587.3348149.6616
1610.4474-0.53320.43470.5954-0.57410.5464-0.2155-0.463-0.01540.09440.4508-0.177-0.07170.15990.16280.25720.0383-0.02730.3951-0.15760.354449.7374116.0904149.6613
162-0.04570.12090.09670.44920.05420.1949-0.0144-0.06210.00650.15740.0725-0.1818-0.0830.07090.00090.23250.0448-0.05280.3721-0.10030.423650.942995.7289144.2677
1630.085-0.0178-0.06030.01720.01210.0192-0.2686-0.1375-0.37860.24780.19060.03330.1161-0.0567-0.00010.39740.0562-0.01150.404-0.03740.439524.925877.8271160.7057
1640.17870.20890.01090.36560.21890.30450.0541-0.0176-0.013-0.02460.0519-0.1465-0.06320.1321-00.23380.0587-0.02710.3487-0.07180.397849.979291.272141.0668
1650.15750.0541-0.0570.059-0.07740.2988-0.0645-0.15530.39360.3195-0.21370.27110.0858-0.2463-0.02280.28920.0724-0.02840.2574-0.09840.348442.938104.1178152.1559
1660.083-0.1125-0.07470.19050.00290.24530.3001-0.3454-0.34070.28280.04170.0123-0.0332-0.03790.00430.3302-0.04860.09040.447-0.03460.39450.613106.4518112.0747
1670.0009-0.007-0.00240.0893-0.01440.0031-0.14270.03810.2279-0.06080.07850.0451-0.6116-0.482-0.00010.50820.02960.03740.7223-0.11420.687751.923196.9038118.1627
1680.10180.11670.06330.29040.19360.49510.02930.0061-0.0749-0.09480.0255-0.0996-0.07230.0682-00.3151-0.01440.110.403-0.05320.507751.43111.9537112.2072
1690.04160.05760.04830.06210.0580.03340.1674-0.55340.4165-0.1248-0.1974-0.14080.13540.29550.00010.3421-0.02760.04140.3829-0.09810.506958.888192.6834110.5147
1700.0131-0.01320.00040.056-0.03270.0163-0.08830.20920.3377-0.11250.10930.0677-0.006-0.01560.00010.3671-0.02170.05450.3838-0.11280.483852.6575103.951104.6683
1710.0285-0.0956-0.01310.2504-0.10290.0316-0.0948-0.0284-0.19580.03580.0164-0.31590.01090.0311-0.09790.2836-0.0410.06970.3367-0.14680.4957.4642117.4777126.5091
1720.07880.0463-0.08080.1496-0.21080.23250.12360.0116-0.2867-0.06160.2321-0.49960.02890.3730.0020.287-0.01780.00320.4839-0.1890.553756.5491120.7493136.0219
1730.5331-0.1439-0.05250.4013-0.34640.2683-0.0189-0.02380.1442-0.06910.0788-0.23-0.09680.14170.00030.2548-0.07370.11110.3487-0.090.44959.9818122.6313112.0695
1740.0233-0.0016-0.04020.0503-0.01040.0187-0.1591-0.0112-0.0705-0.3310.10540.12070.1608-0.1984-0.00030.3968-0.03190.10030.4013-0.09050.501357.910190.329999.147
1750.34420.06870.11350.3550.18810.4570.00190.01450.1434-0.14160.1206-0.1369-0.10180.1063-00.3069-0.05240.14120.3348-0.07840.488156.7731122.4147109.3176
1760.1070.0450.3380.1821-0.08411.28740.0464-0.3015-0.23530.1403-0.053-0.410.5508-0.33770.02710.2358-0.02670.03380.379-0.07580.386257.99111.3936124.1755
1770.0262-0.10440.06170.402-0.18190.16320.10210.02580.2328-0.5051-0.1873-0.06180.1832-0.14220.00660.2460.0683-0.00560.3138-0.09060.382939.611671.0169130.7495
1780.3094-0.22160.16490.1411-0.10150.0882-0.3191-0.0566-0.2066-0.45370.0551-0.3362-0.2255-0.9285-0.02030.68410.11930.00660.7934-0.14980.69835.098977.2105117.1938
1790.02810.00940.05410.00430.02320.08120.0381-0.0113-0.1789-0.14560.108-0.2956-0.0626-0.19970.00020.32790.07140.00460.427-0.11420.513144.229363.1892121.2301
1800.35820.4818-0.11050.5569-0.0560.05820.1120.02540.1769-0.0262-0.0886-0.1264-0.1381-0.0883-00.2550.0682-0.02450.3397-0.0660.329327.739477.9987135.0782
1810.11870.18090.01880.28350.09330.0529-0.01820.1986-0.2374-0.23430.1418-0.12640.00220.1249-0.00550.24730.05550.04660.3724-0.10160.454550.588669.8971122.4058
1820.03570.1351-0.0990.5035-0.02580.20920.0204-0.11720.0214-0.29950.1141-0.0855-0.00320.07270.02080.23830.08070.02310.3073-0.10670.455541.827572.3308132.9663
1830.070.07290.05280.04870.11480.29740.07740.04010.0195-0.04750.0485-0.420.15180.2525-0.00010.26390.0899-0.03290.3273-0.05470.362424.531352.1648127.8055
1840.1695-0.2569-0.17290.34320.23290.476-0.02420.0186-0.17360.10680.0785-0.14170.11180.10300.22640.0667-0.07540.302-0.05820.358337.720465.5665142.9101
1850.04510.0563-0.00060.05050.00380.275-0.16590.34990.1008-0.3206-0.1218-0.4736-0.21130.3323-0.00110.38250.02970.04210.3947-0.07890.530456.207784.7008120.4038
1860.17540.11260.04190.7503-0.05470.4290.0344-0.0794-0.10590.13060.0328-0.10340.0016-0.03760.00390.20490.0647-0.04740.3043-0.06370.286135.269668.8085143.2584
1870.0059-0.0391-0.0730.0516-0.00810.13160.05170.2903-0.363-0.4794-0.0598-0.00820.14330.11570.00030.30720.0561-0.05730.3493-0.12150.380134.74460.0259127.3324
1880.20710.16670.040.12660.10080.11950.2766-0.07840.7422-0.20920.0438-0.0018-0.45130.4154-0.01610.36940.04060.14010.3981-0.09820.439437.072279.056989.5476
1890.08030.11140.05260.1150.05160.0310.04340.05960.06740.16790.02030.02640.05580.0406-0.00020.44840.01460.08920.4032-0.04480.578946.641984.071989.0862
1900.16160.0280.00440.0797-0.15160.1946-0.02030.0090.2003-0.2030.01970.0947-0.1478-0.1603-00.35530.0416-0.00210.3924-0.06630.387321.743377.381685.7983
1910.0683-0.00730.06930.05220.0160.0495-0.1699-0.1528-0.0057-0.01370.1419-0.2073-0.00080.020900.29320.040.13110.3644-0.05320.418648.055674.80584.7329
1920.0180.01720.02490.02080.00720.0890.2330.4729-0.2357-0.2443-0.1396-0.4115-0.1549-0.33490.00020.35730.01810.01090.3985-0.03660.404350.651877.322497.7921
1930.0720.04170.06240.03690.00820.08550.05050.2275-0.1454-0.0371-0.33680.1270.0367-0.0721-00.29350.05290.05840.4038-0.03520.428838.343672.261992.8697
1940.09950.032-0.04280.0343-0.00260.0043-0.14360.10830.12-0.01420.1615-0.21660.0357-0.08360.00130.47570.02090.11190.4973-0.0110.365141.065589.062666.208
1950.49960.0121-0.14920.23770.21950.61580.0650.1651-0.005-0.0973-0.0919-0.2278-0.03610.0108-0.01610.31110.0690.05880.3684-0.07830.228734.683672.99273.1512
19600.04360.03960.08730.10480.07890.1297-0.16270.20780.31360.0906-0.2070.07360.08520.00040.3150.05920.05190.3612-0.07310.419849.16168.8389105.2908
1970.48230.1846-0.05830.0619-0.00320.5105-0.01680.1796-0.0565-0.1532-0.0418-0.09220.0253-0.052900.29080.07060.03580.3605-0.09050.28831.066169.511475.7423
1980.02060.0352-0.0370.03870.02710.01520.16520.1290.16010.30520.1066-0.3225-0.18770.57010.00030.45760.00010.10050.5151-0.05430.491242.495884.223777.3339
1990.0394-0.0342-0.04290.02330.05670.14920.03110.0709-0.0332-0.19160.0190.0853-0.01050.2185-00.42010.0958-0.03910.34210.00510.3715-33.8772148.0611121.1922
2000.0616-0.05380.04210.05290.04690.0979-0.08030.16560.1978-0.15790.3166-0.21730.04520.5301-0.00060.68030.1563-0.02850.732-0.10510.5506-35.2723136.2988112.4609
2010.22240.1465-0.30910.3511-0.2160.35810.0443-0.06010.1236-0.0366-0.072-0.0032-0.2310.0638-00.4060.0764-0.02340.3501-0.05880.3592-24.8837147.0503121.0166
2020.1050.0715-0.01920.0461-0.01410.0320.09990.0275-0.2871-0.37170.17980.3531-0.03840.12340.01250.41260.1051-0.03850.379-0.0080.3399-27.8645142.0284121.3646
2030.07750.0909-0.1170.0711-0.09770.06550.04190.0244-0.0859-0.615-0.12620.099-0.085-0.2395-0.00020.43050.0818-0.09310.3628-0.02650.4755-47.6448145.1623118.114
2040.1720.03180.20770.0140.00180.2011-0.046-0.04270.0980.28730.1207-0.0645-0.0623-0.1193-0.00010.37280.0947-0.04330.30860.01690.4102-35.0045148.4464124.3248
2050.1219-0.0096-0.0737-0.00650.0160.12410.03160.053-0.0581-0.03150.1010.2186-0.2125-0.4255-0.00010.53030.1107-0.02820.33880.0210.413-22.7386160.6562102.9591
2060.6691-0.31520.37230.1399-0.14270.31660.04280.08230.1703-0.0169-0.05990.088-0.1172-0.04230.00010.40590.06410.00950.2702-0.02320.3953-27.4581159.6761126.394
2070.0220.0295-0.02820.02210.0026-0.0001-0.0360.1595-0.25220.2136-0.13860.35320.5071-0.2161-0.00020.46750.0053-0.04060.4311-0.09120.4627-51.5146134.0797127.2444
2080.1867-0.20280.05570.5374-0.03310.34380.05380.09380.1381-0.0362-0.03970.0074-0.17180.03480.00010.35220.0692-0.00350.2725-0.03550.3465-25.2143156.5393127.9458
2090.06690.01270.06270.01520.00850.03640.26050.33180.2374-0.1807-0.0760.37330.0253-0.042-0.00030.62160.1055-0.07050.3750.04870.4763-31.7411154.3464110.7214
2100.03750.044-0.05950.0745-0.0790.10410.1447-0.1961-0.0895-0.099-0.13710.19470.34240.024-0.00080.39650.0511-0.13190.4439-0.02050.4032-48.4377119.297589.4288
2110.32260.0291-0.05780.12870.00540.13580.0236-0.2913-0.07740.4648-0.40250.09920.2975-0.0092-0.01960.7340.0253-0.03990.98890.21990.9882-39.1874115.6194103.7414
2120.00560.02110.01520.03330.01430.02680.0183-0.0057-0.1801-0.0205-0.068-0.048-0.45080.0584-0.00020.55330.1106-0.14150.4585-0.07080.5948-57.1817116.111100.1671
2130.21320.3591-0.01170.53730.05720.23870.0803-0.0612-0.1976-0.1775-0.12860.0503-0.0952-0.04370.00010.42570.1198-0.14560.3594-0.03050.3401-41.2139116.458287.1444
2140.01910.03640.0280.03330.04080.0607-0.1354-0.0974-0.01530.23220.08440.2258-0.272-0.243100.52430.1201-0.14810.4905-0.12090.5089-56.3461125.5684101.4422
2150.26680.2704-0.30170.3328-0.12430.42610.19260.2720.21450.1104-0.13890.20730.04890.10710.07640.40750.0987-0.17160.3794-0.0590.44-48.651122.374888.0311
2160.07330.1881-0.08160.4334-0.24640.2111-0.09840.0970.1747-0.06720.01540.4585-0.2816-0.50270.0160.36650.1011-0.20510.4542-0.09050.4213-53.42594.699784.1515
2170.16190.0637-0.17860.4303-0.0470.28790.1640.1429-0.0563-0.1211-0.17920.6296-0.0649-0.03540.63010.47480.1946-0.34610.4372-0.03280.3013-48.8215116.986175.9256
2180.1358-0.052-0.0540.03460.06590.1454-0.1041-0.09210.24020.1908-0.1287-0.0601-0.5338-0.0801-0.00370.51080.124-0.12410.4293-0.01770.4558-52.5413137.1371102.3524
2191.03280.2414-0.03030.58040.00810.2481-0.110.1595-0.0691-0.1761-0.07530.1716-0.0757-0.0755-0.35870.40870.1424-0.20440.3826-0.00880.2713-44.385117.038775.0687
2200.02910.0032-0.0379-0.0070.00120.0675-0.0516-0.3503-0.0070.1377-0.14570.116-0.2333-0.4911-0.00040.5140.0631-0.14520.4715-0.02060.5956-53.5348107.97689.0064
2210.05720.03470.06030.06660.08670.10530.1019-0.1893-0.0053-0.2956-0.220.0352-0.14690.20290.00010.61220.0879-0.12180.41080.05890.3998-29.3672137.041578.4513
2220.08480.0389-0.01980.0661-0.05960.0528-0.1182-0.4272-0.4816-0.1987-0.266-0.3106-0.08910.2962-0.00590.66580.0375-0.01340.87910.14370.6899-16.0919130.511377.5004
2230.08120.19390.13270.47140.30390.21070.13530.03520.0029-0.1181-0.1850.106-0.03890.06010.00010.49570.1359-0.10150.4687-0.00330.3809-28.0985137.352386.1195
2240.0214-0.0399-0.03030.07560.04620.0137-0.10820.1098-0.1993-0.1920.0029-0.46850.20770.1530.00050.57850.0701-0.12410.4140.02530.4591-26.6388131.55985.178
225-0.00360.04470.03580.14660.08710.0389-0.05050.4480.2205-0.45940.0124-0.2887-0.37840.08620.00120.71330.1414-0.05520.54710.05920.3823-26.2542136.441664.6767
2260.0182-0.0032-0.01730.0353-0.01530.0213-0.1123-0.16220.1425-0.32060.36730.0608-0.1592-0.26670.00020.54980.0895-0.12370.40360.02480.3294-30.4782128.98975.9423
2270.24220.1171-0.11680.0194-0.07580.16650.12860.30660.3898-0.1782-0.10530.1482-0.05650.16340.02260.57630.1454-0.03830.40610.03170.3615-24.6957153.027584.51
2280.5594-0.10780.11610.1006-0.13210.07830.03340.11340.1247-0.1682-0.05420.1277-0.1680.01620.00290.50040.1164-0.090.32210.04470.3778-33.3472149.877386.0316
2291.4040.4915-0.40790.6162-0.24710.1469-0.04680.3518-0.4045-0.649-0.2097-0.2374-0.0325-0.1587-0.09920.6730.1204-0.15480.5558-0.00810.3833-29.3717121.827361.2603
2300.3203-0.01790.01110.59720.04270.25850.07470.10450.0873-0.0957-0.0330.1776-0.15440.050.04730.49060.1228-0.10990.39440.02350.3255-39.0903142.414887.3262
2310.0144-0.0262-0.01610.0304-0.01350.019-0.01790.06250.2968-0.1438-0.2488-0.7664-0.4415-0.10520.00060.6070.0118-0.01230.47340.1090.5536-23.079148.281279.7763
2320.0964-0.12580.05550.1835-0.02050.07080.12690.0402-0.46380.1818-0.2599-0.28180.3451-0.042-0.00770.69370.05510.03360.57610.04140.36957.5999123.834666.1923
2330.00620.0079-0.01540.02990.03410.0488-0.1198-0.0532-0.0138-0.2441-0.1876-0.16870.1397-0.06580.00110.80540.14570.02820.63730.02030.36384.1296117.96457.6879
2340.1339-0.14440.04270.12270.00750.06240.0529-0.24750.0103-0.1062-0.1113-0.3450.07450.125500.560.02810.06830.43740.03760.401820.5082126.897777.619
2350.08080.03050.02880.08980.03840.02320.24160.1495-0.0532-0.2235-0.1486-0.06730.1186-0.49620.00070.68910.05680.05490.47060.06770.366110.4495124.683770.233
2360.0665-0.08040.01160.0404-0.02460.00550.0333-0.0209-0.0507-0.7866-0.04750.19490.14590.0236-0.00020.78240.07920.01260.61720.07330.4007-0.3025126.345753.0227
2370.13490.15560.04570.19150.05720.01530.24990.039-0.0464-0.1069-0.12460.0331-0.34910.009-0.00010.65820.11590.12460.54730.02730.30217.964130.878362.8213
2380.107-0.00350.04130.1319-0.08320.08210.17260.17480.1765-0.6438-0.1018-0.0872-0.23440.14490.0030.70570.08230.16160.640.06090.33127.3189107.575154.8689
2390.4109-0.48660.06320.7692-0.11740.0340.22760.4814-0.1453-0.6191-0.19090.28-0.12510.14950.19790.5570.06780.34380.45330.1443-0.007423.6067127.998760.6141
2400.0680.08050.01250.05830.01880.0426-0.04210.28970.2733-0.11390.19480.64310.12970.21530.00060.64720.1127-0.01630.63160.0660.4333-10.6185134.644559.5308
2410.1056-0.1701-0.24120.58830.37560.4670.09980.06470.0195-0.22630.0309-0.1725-0.0780.1280.01810.61650.0080.1620.43890.10840.342824.0833131.951564.3854
2420.0185-0.0002-0.01790.02260.02480.0292-0.05230.6081-0.5226-0.2621-0.08480.2510.0413-0.0139-00.75880.08540.08490.6129-0.07060.396716.4784116.96157.8897
2430.111-0.0639-0.11190.08340.14020.20230.2566-0.08580.22630.4693-0.01240.3395-0.3374-0.2190.00580.6829-0.01370.1490.3720.10380.401814.1523144.401784.3083
2440.05130.0080.04810.0159-0.01590.0347-0.03050.2837-0.15810.0431-0-0.0372-0.0592-0.077400.7732-0.05490.17280.49080.05090.583418.719152.990789.4792
2450.4325-0.3136-0.04370.21970.0468-0.00710.2233-0.0592-0.1792-0.0984-0.08820.1629-0.2335-0.16230.03460.55760.05710.04230.41360.04340.276-0.4882136.582179.0018
2460.0204-0.05160.01860.14860.01560.11150.316-0.28090.3411-0.0578-0.1404-0.1009-0.2249-0.154-0.00410.6228-0.01850.10630.44860.04720.41169.8357138.928483.4463
2470.0862-0.00820.11330.00760.03190.1037-0.02970.16320.1121-0.09680.119-0.2866-0.32140.3955-00.6671-0.01060.17080.48240.05740.541925.8685153.882482.3899
2480.09260.03390.14330.03820.0630.1244-0.0307-0.1245-0.0812-0.49540.1646-0.1753-0.12920.16780.00010.67250.02230.14380.43640.06460.451416.9738145.717877.0993
2490.24790.09690.04220.01140.01740.1047-0.014-0.15130.2276-0.2624-0.17750.0287-0.53210.2170.00070.65360.04620.03610.37510.08830.462-4.0252164.815190.4298
2500.09690.1419-0.0440.32140.09780.30960.12320.09010.1997-0.2733-0.03440.0468-0.1498-0.06780.0120.5870.07180.07420.36120.12250.30751.9594153.064174.0055
2510.0525-0.009-0.022-0.0106-0.00790.01270.10380.1718-0.0116-0.169-0.12-0.11570.22790.2741-0.00030.64920.02950.15610.53060.04540.51935.6468142.766878.7684
2520.3599-0.1813-0.23740.63080.07690.12340.08520.01640.1719-0.1788-0.1015-0.055-0.171-0.0205-0.00720.63390.06290.08890.41760.13190.26352.2798148.253271.0028
2530.0399-0.00960.07080.0128-0.02090.0595-0.0748-0.02350.04420.3569-0.0069-0.1255-0.18010.27180.00010.759-0.01240.0950.49070.00090.48757.4675157.53886.3489
2540.03730.04540.02790.18130.0840.05220.14190.08110.07360.077-0.1372-0.084-0.208-0.07580.00020.30730.01680.00030.3164-0.06550.3464-51.0663107.8309133.0724
2550.2233-0.0232-0.10810.01180.01260.0083-0.17840.0089-0.2775-0.11850.172-0.646-0.0588-0.02890.00390.55630.0234-0.07050.5278-0.14370.8106-42.4523118.1835127.3194
2560.2596-0.06940.34780.11090.03330.5639-0.04090.05650.11270.18750.0104-0.04790.0662-0.0769-00.2728-0.0137-0.02510.2919-0.03350.4046-43.7851102.7845134.8329
2570.0179-0.05890.00990.0602-0.02190.0690.30990.1430.1103-0.231-0.1937-0.0837-0.4289-0.0666-00.3335-0.0003-0.01920.3826-0.07840.4731-43.5581105.5544129.6032
2580.02230.05510.03060.0685-0.04780.11410.10930.0060.2629-0.0568-0.03110.3822-0.11430.0817-0.00010.40040.0702-0.03050.4103-0.03830.4596-58.6053119.2176128.3881
2590.0237-0.0507-0.04340.370.04880.0228-0.0590.0452-0.1281-0.0828-0.03130.2188-0.0468-0.1668-00.28470.05370.00020.386-0.07860.3716-53.452106.015131.5214
2600.12570.05280.17490.26460.04050.1272-0.0880.027-0.02560.05210.01330.2395-0.08430.0379-0.00010.28860.02250.06070.3063-0.04270.3433-41.3965111.5239155.0275
2610.4315-0.13190.04760.73030.19750.0862-0.0288-0.0250.01960.0493-0.03120.2015-0.0519-0.0423-0.00020.238-0.00660.02990.2954-0.0420.3705-55.022697.6597140.6789
2620.01930.0236-0.01690.0522-0.03210.0272-0.06860.0410.4066-0.29320.22190.2848-0.0212-0.00220.00010.45930.023-0.11730.4273-0.06430.4771-58.7473118.0825112.9655
2630.30510.1223-0.22810.27760.18660.47430.0043-0.0605-0.09090.0267-0.06380.15390.0142-0.1226-0.00120.24010.00570.00320.2971-0.0710.3728-52.023395.7019138.7846
2640.25560.33790.2490.48580.11951.78050.03130.1540.4776-0.26870.23950.1547-0.67490.25580.08160.30680.0260.00410.2498-0.1520.3496-48.3929112.6845144.3365
精密化 TLSグループ
IDRefine-IDRefine TLS-IDSelection detailsAuth asym-IDAuth seq-ID
1X-RAY DIFFRACTION1(chain A and resid 4:24)A4 - 24
2X-RAY DIFFRACTION2(chain A and resid 25:47)A25 - 47
3X-RAY DIFFRACTION3(chain A and resid 48:75)A48 - 75
4X-RAY DIFFRACTION4(chain A and resid 76:82)A76 - 82
5X-RAY DIFFRACTION5(chain A and resid 83:105)A83 - 105
6X-RAY DIFFRACTION6(chain A and resid 106:128)A106 - 128
7X-RAY DIFFRACTION7(chain A and resid 129:157)A129 - 157
8X-RAY DIFFRACTION8(chain A and resid 158:211)A158 - 211
9X-RAY DIFFRACTION9(chain A and resid 212:232)A212 - 232
10X-RAY DIFFRACTION10(chain A and resid 233:299)A233 - 299
11X-RAY DIFFRACTION11(chain A and resid 300:313)A300 - 313
12X-RAY DIFFRACTION12(chain B and resid 4:18)B4 - 18
13X-RAY DIFFRACTION13(chain B and resid 19:28)B19 - 28
14X-RAY DIFFRACTION14(chain B and resid 29:41)B29 - 41
15X-RAY DIFFRACTION15(chain B and resid 42:88)B42 - 88
16X-RAY DIFFRACTION16(chain B and resid 89:105)B89 - 105
17X-RAY DIFFRACTION17(chain B and resid 106:125)B106 - 125
18X-RAY DIFFRACTION18(chain B and resid 126:147)B126 - 147
19X-RAY DIFFRACTION19(chain B and resid 148:211)B148 - 211
20X-RAY DIFFRACTION20(chain B and resid 212:232)B212 - 232
21X-RAY DIFFRACTION21(chain B and resid 233:299)B233 - 299
22X-RAY DIFFRACTION22(chain B and resid 300:313)B300 - 313
23X-RAY DIFFRACTION23(chain C and resid 4:24)C4 - 24
24X-RAY DIFFRACTION24(chain C and resid 25:47)C25 - 47
25X-RAY DIFFRACTION25(chain C and resid 48:68)C48 - 68
26X-RAY DIFFRACTION26(chain C and resid 69:79)C69 - 79
27X-RAY DIFFRACTION27(chain C and resid 80:105)C80 - 105
28X-RAY DIFFRACTION28(chain C and resid 106:125)C106 - 125
29X-RAY DIFFRACTION29(chain C and resid 126:160)C126 - 160
30X-RAY DIFFRACTION30(chain C and resid 161:213)C161 - 213
31X-RAY DIFFRACTION31(chain C and resid 214:232)C214 - 232
32X-RAY DIFFRACTION32(chain C and resid 233:299)C233 - 299
33X-RAY DIFFRACTION33(chain C and resid 300:313)C300 - 313
34X-RAY DIFFRACTION34(chain D and resid 4:24)D4 - 24
35X-RAY DIFFRACTION35(chain D and resid 25:42)D25 - 42
36X-RAY DIFFRACTION36(chain D and resid 43:86)D43 - 86
37X-RAY DIFFRACTION37(chain D and resid 87:105)D87 - 105
38X-RAY DIFFRACTION38(chain D and resid 106:117)D106 - 117
39X-RAY DIFFRACTION39(chain D and resid 118:136)D118 - 136
40X-RAY DIFFRACTION40(chain D and resid 137:147)D137 - 147
41X-RAY DIFFRACTION41(chain D and resid 148:211)D148 - 211
42X-RAY DIFFRACTION42(chain D and resid 212:232)D212 - 232
43X-RAY DIFFRACTION43(chain D and resid 233:299)D233 - 299
44X-RAY DIFFRACTION44(chain D and resid 300:313)D300 - 313
45X-RAY DIFFRACTION45(chain E and resid 4:18)E4 - 18
46X-RAY DIFFRACTION46(chain E and resid 19:36)E19 - 36
47X-RAY DIFFRACTION47(chain E and resid 37:68)E37 - 68
48X-RAY DIFFRACTION48(chain E and resid 69:79)E69 - 79
49X-RAY DIFFRACTION49(chain E and resid 80:105)E80 - 105
50X-RAY DIFFRACTION50(chain E and resid 106:122)E106 - 122
51X-RAY DIFFRACTION51(chain E and resid 123:147)E123 - 147
52X-RAY DIFFRACTION52(chain E and resid 148:212)E148 - 212
53X-RAY DIFFRACTION53(chain E and resid 213:230)E213 - 230
54X-RAY DIFFRACTION54(chain E and resid 231:300)E231 - 300
55X-RAY DIFFRACTION55(chain E and resid 301:313)E301 - 313
56X-RAY DIFFRACTION56(chain F and resid 4:20)F4 - 20
57X-RAY DIFFRACTION57(chain F and resid 21:40)F21 - 40
58X-RAY DIFFRACTION58(chain F and resid 41:88)F41 - 88
59X-RAY DIFFRACTION59(chain F and resid 89:105)F89 - 105
60X-RAY DIFFRACTION60(chain F and resid 106:119)F106 - 119
61X-RAY DIFFRACTION61(chain F and resid 120:147)F120 - 147
62X-RAY DIFFRACTION62(chain F and resid 148:211)F148 - 211
63X-RAY DIFFRACTION63(chain F and resid 212:232)F212 - 232
64X-RAY DIFFRACTION64(chain F and resid 233:295)F233 - 295
65X-RAY DIFFRACTION65(chain F and resid 296:309)F296 - 309
66X-RAY DIFFRACTION66(chain F and resid 310:313)F310 - 313
67X-RAY DIFFRACTION67(chain G and resid 4:18)G4 - 18
68X-RAY DIFFRACTION68(chain G and resid 19:35)G19 - 35
69X-RAY DIFFRACTION69(chain G and resid 36:77)G36 - 77
70X-RAY DIFFRACTION70(chain G and resid 78:88)G78 - 88
71X-RAY DIFFRACTION71(chain G and resid 89:105)G89 - 105
72X-RAY DIFFRACTION72(chain G and resid 106:127)G106 - 127
73X-RAY DIFFRACTION73(chain G and resid 128:157)G128 - 157
74X-RAY DIFFRACTION74(chain G and resid 158:211)G158 - 211
75X-RAY DIFFRACTION75(chain G and resid 212:230)G212 - 230
76X-RAY DIFFRACTION76(chain G and resid 231:299)G231 - 299
77X-RAY DIFFRACTION77(chain G and resid 300:313)G300 - 313
78X-RAY DIFFRACTION78(chain H and resid 4:23)H4 - 23
79X-RAY DIFFRACTION79(chain H and resid 24:39)H24 - 39
80X-RAY DIFFRACTION80(chain H and resid 40:68)H40 - 68
81X-RAY DIFFRACTION81(chain H and resid 69:79)H69 - 79
82X-RAY DIFFRACTION82(chain H and resid 80:105)H80 - 105
83X-RAY DIFFRACTION83(chain H and resid 106:126)H106 - 126
84X-RAY DIFFRACTION84(chain H and resid 127:159)H127 - 159
85X-RAY DIFFRACTION85(chain H and resid 160:211)H160 - 211
86X-RAY DIFFRACTION86(chain H and resid 212:232)H212 - 232
87X-RAY DIFFRACTION87(chain H and resid 233:299)H233 - 299
88X-RAY DIFFRACTION88(chain H and resid 300:313)H300 - 313
89X-RAY DIFFRACTION89(chain I and resid 4:24)I4 - 24
90X-RAY DIFFRACTION90(chain I and resid 25:47)I25 - 47
91X-RAY DIFFRACTION91(chain I and resid 48:68)I48 - 68
92X-RAY DIFFRACTION92(chain I and resid 69:79)I69 - 79
93X-RAY DIFFRACTION93(chain I and resid 80:105)I80 - 105
94X-RAY DIFFRACTION94(chain I and resid 106:122)I106 - 122
95X-RAY DIFFRACTION95(chain I and resid 123:147)I123 - 147
96X-RAY DIFFRACTION96(chain I and resid 148:211)I148 - 211
97X-RAY DIFFRACTION97(chain I and resid 212:233)I212 - 233
98X-RAY DIFFRACTION98(chain I and resid 234:299)I234 - 299
99X-RAY DIFFRACTION99(chain I and resid 300:313)I300 - 313
100X-RAY DIFFRACTION100(chain J and resid 4:17)J4 - 17
101X-RAY DIFFRACTION101(chain J and resid 18:28)J18 - 28
102X-RAY DIFFRACTION102(chain J and resid 29:41)J29 - 41
103X-RAY DIFFRACTION103(chain J and resid 42:89)J42 - 89
104X-RAY DIFFRACTION104(chain J and resid 90:105)J90 - 105
105X-RAY DIFFRACTION105(chain J and resid 106:126)J106 - 126
106X-RAY DIFFRACTION106(chain J and resid 127:147)J127 - 147
107X-RAY DIFFRACTION107(chain J and resid 148:211)J148 - 211
108X-RAY DIFFRACTION108(chain J and resid 212:233)J212 - 233
109X-RAY DIFFRACTION109(chain J and resid 234:299)J234 - 299
110X-RAY DIFFRACTION110(chain J and resid 300:313)J300 - 313
111X-RAY DIFFRACTION111(chain K and resid 4:17)K4 - 17
112X-RAY DIFFRACTION112(chain K and resid 18:36)K18 - 36
113X-RAY DIFFRACTION113(chain K and resid 37:68)K37 - 68
114X-RAY DIFFRACTION114(chain K and resid 69:79)K69 - 79
115X-RAY DIFFRACTION115(chain K and resid 80:105)K80 - 105
116X-RAY DIFFRACTION116(chain K and resid 106:124)K106 - 124
117X-RAY DIFFRACTION117(chain K and resid 125:147)K125 - 147
118X-RAY DIFFRACTION118(chain K and resid 148:211)K148 - 211
119X-RAY DIFFRACTION119(chain K and resid 212:232)K212 - 232
120X-RAY DIFFRACTION120(chain K and resid 233:299)K233 - 299
121X-RAY DIFFRACTION121(chain K and resid 300:313)K300 - 313
122X-RAY DIFFRACTION122(chain L and resid 4:16)L4 - 16
123X-RAY DIFFRACTION123(chain L and resid 17:37)L17 - 37
124X-RAY DIFFRACTION124(chain L and resid 38:68)L38 - 68
125X-RAY DIFFRACTION125(chain L and resid 69:81)L69 - 81
126X-RAY DIFFRACTION126(chain L and resid 82:105)L82 - 105
127X-RAY DIFFRACTION127(chain L and resid 106:117)L106 - 117
128X-RAY DIFFRACTION128(chain L and resid 118:136)L118 - 136
129X-RAY DIFFRACTION129(chain L and resid 137:211)L137 - 211
130X-RAY DIFFRACTION130(chain L and resid 212:232)L212 - 232
131X-RAY DIFFRACTION131(chain L and resid 233:299)L233 - 299
132X-RAY DIFFRACTION132(chain L and resid 300:313)L300 - 313
133X-RAY DIFFRACTION133(chain M and resid 4:18)M4 - 18
134X-RAY DIFFRACTION134(chain M and resid 19:36)M19 - 36
135X-RAY DIFFRACTION135(chain M and resid 37:68)M37 - 68
136X-RAY DIFFRACTION136(chain M and resid 69:79)M69 - 79
137X-RAY DIFFRACTION137(chain M and resid 80:105)M80 - 105
138X-RAY DIFFRACTION138(chain M and resid 106:122)M106 - 122
139X-RAY DIFFRACTION139(chain M and resid 123:147)M123 - 147
140X-RAY DIFFRACTION140(chain M and resid 148:211)M148 - 211
141X-RAY DIFFRACTION141(chain M and resid 212:232)M212 - 232
142X-RAY DIFFRACTION142(chain M and resid 233:299)M233 - 299
143X-RAY DIFFRACTION143(chain M and resid 300:313)M300 - 313
144X-RAY DIFFRACTION144(chain N and resid 4:24)N4 - 24
145X-RAY DIFFRACTION145(chain N and resid 25:38)N25 - 38
146X-RAY DIFFRACTION146(chain N and resid 39:90)N39 - 90
147X-RAY DIFFRACTION147(chain N and resid 91:105)N91 - 105
148X-RAY DIFFRACTION148(chain N and resid 106:117)N106 - 117
149X-RAY DIFFRACTION149(chain N and resid 118:134)N118 - 134
150X-RAY DIFFRACTION150(chain N and resid 135:149)N135 - 149
151X-RAY DIFFRACTION151(chain N and resid 150:211)N150 - 211
152X-RAY DIFFRACTION152(chain N and resid 212:232)N212 - 232
153X-RAY DIFFRACTION153(chain N and resid 233:299)N233 - 299
154X-RAY DIFFRACTION154(chain N and resid 300:313)N300 - 313
155X-RAY DIFFRACTION155(chain O and resid 5:18)O5 - 18
156X-RAY DIFFRACTION156(chain O and resid 19:36)O19 - 36
157X-RAY DIFFRACTION157(chain O and resid 37:67)O37 - 67
158X-RAY DIFFRACTION158(chain O and resid 68:79)O68 - 79
159X-RAY DIFFRACTION159(chain O and resid 80:105)O80 - 105
160X-RAY DIFFRACTION160(chain O and resid 106:122)O106 - 122
161X-RAY DIFFRACTION161(chain O and resid 123:147)O123 - 147
162X-RAY DIFFRACTION162(chain O and resid 148:211)O148 - 211
163X-RAY DIFFRACTION163(chain O and resid 212:232)O212 - 232
164X-RAY DIFFRACTION164(chain O and resid 233:299)O233 - 299
165X-RAY DIFFRACTION165(chain O and resid 300:313)O300 - 313
166X-RAY DIFFRACTION166(chain P and resid 4:24)P4 - 24
167X-RAY DIFFRACTION167(chain P and resid 25:38)P25 - 38
168X-RAY DIFFRACTION168(chain P and resid 39:89)P39 - 89
169X-RAY DIFFRACTION169(chain P and resid 90:105)P90 - 105
170X-RAY DIFFRACTION170(chain P and resid 106:118)P106 - 118
171X-RAY DIFFRACTION171(chain P and resid 119:136)P119 - 136
172X-RAY DIFFRACTION172(chain P and resid 137:157)P137 - 157
173X-RAY DIFFRACTION173(chain P and resid 158:210)P158 - 210
174X-RAY DIFFRACTION174(chain P and resid 211:232)P211 - 232
175X-RAY DIFFRACTION175(chain P and resid 233:300)P233 - 300
176X-RAY DIFFRACTION176(chain P and resid 301:313)P301 - 313
177X-RAY DIFFRACTION177(chain Q and resid 4:18)Q4 - 18
178X-RAY DIFFRACTION178(chain Q and resid 19:33)Q19 - 33
179X-RAY DIFFRACTION179(chain Q and resid 34:46)Q34 - 46
180X-RAY DIFFRACTION180(chain Q and resid 47:79)Q47 - 79
181X-RAY DIFFRACTION181(chain Q and resid 80:105)Q80 - 105
182X-RAY DIFFRACTION182(chain Q and resid 106:125)Q106 - 125
183X-RAY DIFFRACTION183(chain Q and resid 126:160)Q126 - 160
184X-RAY DIFFRACTION184(chain Q and resid 161:213)Q161 - 213
185X-RAY DIFFRACTION185(chain Q and resid 214:231)Q214 - 231
186X-RAY DIFFRACTION186(chain Q and resid 232:299)Q232 - 299
187X-RAY DIFFRACTION187(chain Q and resid 300:313)Q300 - 313
188X-RAY DIFFRACTION188(chain R and resid 4:24)R4 - 24
189X-RAY DIFFRACTION189(chain R and resid 25:47)R25 - 47
190X-RAY DIFFRACTION190(chain R and resid 48:75)R48 - 75
191X-RAY DIFFRACTION191(chain R and resid 76:90)R76 - 90
192X-RAY DIFFRACTION192(chain R and resid 91:105)R91 - 105
193X-RAY DIFFRACTION193(chain R and resid 106:119)R106 - 119
194X-RAY DIFFRACTION194(chain R and resid 120:147)R120 - 147
195X-RAY DIFFRACTION195(chain R and resid 148:211)R148 - 211
196X-RAY DIFFRACTION196(chain R and resid 212:233)R212 - 233
197X-RAY DIFFRACTION197(chain R and resid 234:299)R234 - 299
198X-RAY DIFFRACTION198(chain R and resid 300:313)R300 - 313
199X-RAY DIFFRACTION199(chain T and resid 4:18)T4 - 18
200X-RAY DIFFRACTION200(chain T and resid 19:36)T19 - 36
201X-RAY DIFFRACTION201(chain T and resid 37:68)T37 - 68
202X-RAY DIFFRACTION202(chain T and resid 69:81)T69 - 81
203X-RAY DIFFRACTION203(chain T and resid 82:105)T82 - 105
204X-RAY DIFFRACTION204(chain T and resid 106:125)T106 - 125
205X-RAY DIFFRACTION205(chain T and resid 126:159)T126 - 159
206X-RAY DIFFRACTION206(chain T and resid 160:211)T160 - 211
207X-RAY DIFFRACTION207(chain T and resid 212:232)T212 - 232
208X-RAY DIFFRACTION208(chain T and resid 233:299)T233 - 299
209X-RAY DIFFRACTION209(chain T and resid 300:313)T300 - 313
210X-RAY DIFFRACTION210(chain U and resid 4:18)U4 - 18
211X-RAY DIFFRACTION211(chain U and resid 19:28)U19 - 28
212X-RAY DIFFRACTION212(chain U and resid 29:42)U29 - 42
213X-RAY DIFFRACTION213(chain U and resid 43:86)U43 - 86
214X-RAY DIFFRACTION214(chain U and resid 87:105)U87 - 105
215X-RAY DIFFRACTION215(chain U and resid 106:125)U106 - 125
216X-RAY DIFFRACTION216(chain U and resid 126:157)U126 - 157
217X-RAY DIFFRACTION217(chain U and resid 158:211)U158 - 211
218X-RAY DIFFRACTION218(chain U and resid 212:236)U212 - 236
219X-RAY DIFFRACTION219(chain U and resid 237:299)U237 - 299
220X-RAY DIFFRACTION220(chain U and resid 300:313)U300 - 313
221X-RAY DIFFRACTION221(chain V and resid 4:18)V4 - 18
222X-RAY DIFFRACTION222(chain V and resid 19:34)V19 - 34
223X-RAY DIFFRACTION223(chain V and resid 35:68)V35 - 68
224X-RAY DIFFRACTION224(chain V and resid 69:80)V69 - 80
225X-RAY DIFFRACTION225(chain V and resid 81:105)V81 - 105
226X-RAY DIFFRACTION226(chain V and resid 106:118)V106 - 118
227X-RAY DIFFRACTION227(chain V and resid 119:136)V119 - 136
228X-RAY DIFFRACTION228(chain V and resid 137:211)V137 - 211
229X-RAY DIFFRACTION229(chain V and resid 212:232)V212 - 232
230X-RAY DIFFRACTION230(chain V and resid 233:299)V233 - 299
231X-RAY DIFFRACTION231(chain V and resid 300:313)V300 - 313
232X-RAY DIFFRACTION232(chain W and resid 4:24)W4 - 24
233X-RAY DIFFRACTION233(chain W and resid 25:47)W25 - 47
234X-RAY DIFFRACTION234(chain W and resid 48:68)W48 - 68
235X-RAY DIFFRACTION235(chain W and resid 69:81)W69 - 81
236X-RAY DIFFRACTION236(chain W and resid 82:105)W82 - 105
237X-RAY DIFFRACTION237(chain W and resid 106:122)W106 - 122
238X-RAY DIFFRACTION238(chain W and resid 123:147)W123 - 147
239X-RAY DIFFRACTION239(chain W and resid 148:213)W148 - 213
240X-RAY DIFFRACTION240(chain W and resid 214:233)W214 - 233
241X-RAY DIFFRACTION241(chain W and resid 234:298)W234 - 298
242X-RAY DIFFRACTION242(chain W and resid 299:313)W299 - 313
243X-RAY DIFFRACTION243(chain Y and resid 4:24)Y4 - 24
244X-RAY DIFFRACTION244(chain Y and resid 25:47)Y25 - 47
245X-RAY DIFFRACTION245(chain Y and resid 48:68)Y48 - 68
246X-RAY DIFFRACTION246(chain Y and resid 69:79)Y69 - 79
247X-RAY DIFFRACTION247(chain Y and resid 80:105)Y80 - 105
248X-RAY DIFFRACTION248(chain Y and resid 106:122)Y106 - 122
249X-RAY DIFFRACTION249(chain Y and resid 123:147)Y123 - 147
250X-RAY DIFFRACTION250(chain Y and resid 148:211)Y148 - 211
251X-RAY DIFFRACTION251(chain Y and resid 212:233)Y212 - 233
252X-RAY DIFFRACTION252(chain Y and resid 234:299)Y234 - 299
253X-RAY DIFFRACTION253(chain Y and resid 300:313)Y300 - 313
254X-RAY DIFFRACTION254(chain Z and resid 4:18)Z4 - 18
255X-RAY DIFFRACTION255(chain Z and resid 19:36)Z19 - 36
256X-RAY DIFFRACTION256(chain Z and resid 37:68)Z37 - 68
257X-RAY DIFFRACTION257(chain Z and resid 69:81)Z69 - 81
258X-RAY DIFFRACTION258(chain Z and resid 82:105)Z82 - 105
259X-RAY DIFFRACTION259(chain Z and resid 106:125)Z106 - 125
260X-RAY DIFFRACTION260(chain Z and resid 126:160)Z126 - 160
261X-RAY DIFFRACTION261(chain Z and resid 161:213)Z161 - 213
262X-RAY DIFFRACTION262(chain Z and resid 214:231)Z214 - 231
263X-RAY DIFFRACTION263(chain Z and resid 232:299)Z232 - 299
264X-RAY DIFFRACTION264(chain Z and resid 300:313)Z300 - 313

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万見について

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お知らせ

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2022年2月9日: EMDBエントリの付随情報ファイルのフォーマットが新しくなりました

EMDBエントリの付随情報ファイルのフォーマットが新しくなりました

  • EMDBのヘッダファイルのバージョン3が、公式のフォーマットとなりました。
  • これまでは公式だったバージョン1.9は、アーカイブから削除されます。

関連情報:EMDBヘッダ

外部リンク:wwPDBはEMDBデータモデルのバージョン3へ移行します

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2020年8月12日: 新型コロナ情報

新型コロナ情報

URL: https://pdbjlvh1.pdbj.org/emnavi/covid19.php

新ページ: EM Navigatorに新型コロナウイルスの特設ページを開設しました。

関連情報:Covid-19情報 / 2020年3月5日: 新型コロナウイルスの構造データ

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2020年3月5日: 新型コロナウイルスの構造データ

新型コロナウイルスの構造データ

関連情報:万見生物種 / 2020年8月12日: 新型コロナ情報

外部リンク:COVID-19特集ページ - PDBj / 今月の分子2020年2月:コロナウイルスプロテーアーゼ

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2019年1月31日: EMDBのIDの桁数の変更

EMDBのIDの桁数の変更

  • EMDBエントリに付与されているアクセスコード(EMDB-ID)は4桁の数字(例、EMD-1234)でしたが、間もなく枯渇します。これまでの4桁のID番号は4桁のまま変更されませんが、4桁の数字を使い切った後に発行されるIDは5桁以上の数字(例、EMD-12345)になります。5桁のIDは2019年の春頃から発行される見通しです。
  • EM Navigator/万見では、接頭語「EMD-」は省略されています。

関連情報:Q: 「EMD」とは何ですか? / 万見/EM NavigatorにおけるID/アクセスコードの表記

外部リンク:EMDB Accession Codes are Changing Soon! / PDBjへお問い合わせ

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2017年7月12日: PDB大規模アップデート

PDB大規模アップデート

  • 新バージョンのPDBx/mmCIF辞書形式に基づくデータがリリースされました。
  • 今回の更新はバージョン番号が4から5になる大規模なもので、全エントリデータの書き換えが行われる「Remediation」というアップデートに該当します。
  • このバージョンアップで、電子顕微鏡の実験手法に関する多くの項目の書式が改定されました(例:em_softwareなど)。
  • EM NavigatorとYorodumiでも、この改定に基づいた表示内容になります。

外部リンク:wwPDB Remediation / OneDepデータ基準に準拠した、より強化された内容のモデル構造ファイルが、PDBアーカイブで公開されました。

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万見 (Yorodumi)

幾万の構造データを、幾万の視点から

  • 万見(Yorodumi)は、EMDB/PDB/SASBDBなどの構造データを閲覧するためのページです。
  • EM Navigatorの詳細ページの後継、Omokage検索のフロントエンドも兼ねています。

関連情報:EMDB / PDB / SASBDB / 3つのデータバンクの比較 / 万見検索 / 2016年8月31日: 新しいEM Navigatorと万見 / 万見文献 / Jmol/JSmol / 機能・相同性情報 / 新しいEM Navigatorと万見の変更点

他の情報も見る