ソフトウェア | 名称 | バージョン | 分類 | NB |
---|
SCALEPACK | | データスケーリング | | MOLREP | | 位相決定 | | REFMAC | refmac_5.2.0019精密化 | | PDB_EXTRACT | 1.7 | データ抽出 | | MOSFLM | | データ削減 | | HKL-2000 | | データスケーリング | | Coot | | モデル構築 | | MolProbity | | モデル構築 | | |
|
---|
精密化 | 構造決定の手法: 分子置換 開始モデル: 2TRX_A 解像度: 2.2→40 Å / Cor.coef. Fo:Fc: 0.95 / Cor.coef. Fo:Fc free: 0.911 / SU B: 17.861 / SU ML: 0.23 / TLS residual ADP flag: LIKELY RESIDUAL / 交差検証法: THROUGHOUT / ESU R: 0.323 / ESU R Free: 0.261 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD
| Rfactor | 反射数 | %反射 | Selection details |
---|
Rfree | 0.291 | 1281 | 9.895 % | RANDOM |
---|
Rwork | 0.223 | - | - | - |
---|
obs | 0.23 | 12946 | 99 % | - |
---|
|
---|
溶媒の処理 | イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.4 Å / 溶媒モデル: MASK BULK SOLVENT |
---|
原子変位パラメータ | Biso mean: 35.99 Å2
| Baniso -1 | Baniso -2 | Baniso -3 |
---|
1- | -5.017 Å2 | -2.508 Å2 | 0 Å2 |
---|
2- | - | -5.017 Å2 | 0 Å2 |
---|
3- | - | - | 7.525 Å2 |
---|
|
---|
精密化ステップ | サイクル: LAST / 解像度: 2.2→40 Å
| タンパク質 | 核酸 | リガンド | 溶媒 | 全体 |
---|
原子数 | 1626 | 0 | 16 | 96 | 1738 |
---|
|
---|
拘束条件 | Refine-ID | タイプ | Dev ideal | Dev ideal target | 数 |
---|
X-RAY DIFFRACTION | r_bond_refined_d0.013 | 0.022 | 1743 | X-RAY DIFFRACTION | r_bond_other_d | | | X-RAY DIFFRACTION | r_angle_refined_deg1.573 | 1.991 | 2379 | X-RAY DIFFRACTION | r_angle_other_deg | | | X-RAY DIFFRACTION | r_dihedral_angle_1_deg9.426 | 5 | 230 | X-RAY DIFFRACTION | r_dihedral_angle_2_deg36.723 | 26.479 | 71 | X-RAY DIFFRACTION | r_dihedral_angle_3_deg16.163 | 15 | 312 | X-RAY DIFFRACTION | r_dihedral_angle_4_deg5.47 | 15 | 3 | X-RAY DIFFRACTION | r_chiral_restr0.08 | 0.2 | 274 | X-RAY DIFFRACTION | r_gen_planes_refined0.005 | 0.02 | 1285 | X-RAY DIFFRACTION | r_gen_planes_other | | | X-RAY DIFFRACTION | r_nbd_refined0.205 | 0.2 | 747 | X-RAY DIFFRACTION | r_nbd_other | | | X-RAY DIFFRACTION | r_nbtor_refined0.304 | 0.2 | 1156 | X-RAY DIFFRACTION | r_nbtor_other | | | X-RAY DIFFRACTION | r_xyhbond_nbd_refined0.166 | 0.2 | 102 | X-RAY DIFFRACTION | r_xyhbond_nbd_other | | | X-RAY DIFFRACTION | r_metal_ion_refined | | | X-RAY DIFFRACTION | r_metal_ion_other | | | X-RAY DIFFRACTION | r_symmetry_vdw_refined0.211 | 0.2 | 22 | X-RAY DIFFRACTION | r_symmetry_vdw_other | | | X-RAY DIFFRACTION | r_symmetry_hbond_refined0.118 | 0.2 | 5 | X-RAY DIFFRACTION | r_symmetry_hbond_other | | | X-RAY DIFFRACTION | r_symmetry_metal_ion_refined | | | X-RAY DIFFRACTION | r_symmetry_metal_ion_other | | | X-RAY DIFFRACTION | r_mcbond_it0.463 | 1.5 | 1127 | X-RAY DIFFRACTION | r_mcbond_other | | | X-RAY DIFFRACTION | r_mcangle_it0.75 | 2 | 1758 | X-RAY DIFFRACTION | r_scbond_it1.369 | 3 | 702 | X-RAY DIFFRACTION | r_scangle_it1.926 | 4.5 | 611 | X-RAY DIFFRACTION | r_rigid_bond_restr | | | X-RAY DIFFRACTION | r_sphericity_free | | | X-RAY DIFFRACTION | r_sphericity_bonded | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | |
|
---|
LS精密化 シェル | 解像度: 2.2→2.26 Å / Total num. of bins used: 20
| Rfactor | 反射数 | %反射 |
---|
Rfree | 0.383 | 93 | - |
---|
Rwork | 0.305 | 861 | - |
---|
obs | - | - | 99.79 % |
---|
|
---|
精密化 TLS | 手法: refined / Refine-ID: X-RAY DIFFRACTION ID | L11 (°2) | L12 (°2) | L13 (°2) | L22 (°2) | L23 (°2) | L33 (°2) | S11 (Å °) | S12 (Å °) | S13 (Å °) | S21 (Å °) | S22 (Å °) | S23 (Å °) | S31 (Å °) | S32 (Å °) | S33 (Å °) | T11 (Å2) | T12 (Å2) | T13 (Å2) | T22 (Å2) | T23 (Å2) | T33 (Å2) | Origin x (Å) | Origin y (Å) | Origin z (Å) |
---|
1 | 5.0732 | -3.4569 | 6.3741 | 2.3571 | -4.3466 | 8.0152 | -0.3683 | 0.3512 | 1.9155 | -0.9352 | -0.0836 | 0.7408 | -1.593 | -0.3281 | 0.4518 | 0.2927 | 0.0139 | -0.0623 | 0.2695 | 0.1237 | 0.2207 | -31.3683 | 87.4121 | 14.532 | 2 | 4.0819 | -1.1547 | 2.7931 | 6.8048 | 0.7044 | 2.2564 | -0.0274 | -0.0678 | 0.3446 | 0.5007 | 0.0288 | 0.5644 | 0.0888 | -0.46 | -0.0014 | 0.2151 | 0.0002 | 0.032 | 0.1776 | 0.0462 | 0.1016 | -31.2163 | 84.402 | 26.127 | 3 | 5.974 | -1.2677 | 0.6224 | 9.382 | 0.992 | 4.0868 | 0.0104 | -0.495 | 0.0072 | 1.139 | -0.051 | 0.9291 | 0.2055 | -0.2122 | 0.0407 | 0.3332 | -0.0169 | 0.1166 | 0.259 | 0.0673 | 0.183 | -34.7588 | 78.7243 | 28.5175 | 4 | 4.6424 | -0.9702 | 2.9069 | 6.3566 | 1.6269 | 2.6325 | 0.0391 | -0.1477 | -0.2805 | 0.4968 | -0.0143 | 1.3153 | 0.3995 | -0.5188 | -0.0247 | 0.243 | -0.0225 | 0.0632 | 0.2059 | 0.086 | 0.179 | -34.9294 | 73.0833 | 25.0888 | 5 | 7.1368 | 1.1737 | -1.1825 | 9.9218 | -1.9172 | 1.256 | 0.2625 | -0.3555 | 0.2297 | 0.0584 | -0.2996 | 0.9096 | 0.0632 | -0.1343 | 0.037 | 0.2101 | 0.0027 | -0.043 | 0.1986 | 0.0649 | 0.1231 | -32.9236 | 72.46 | 18.0442 | 6 | 2.5751 | 0.3544 | 0.7471 | 8.1459 | 1.2331 | 0.3752 | 0.0034 | -0.1112 | 0.2696 | 0.4414 | -0.0351 | -0.5366 | 0.0217 | -0.0063 | 0.0316 | 0.2238 | 0.0065 | -0.0429 | 0.2048 | 0.0808 | 0.1323 | -22.8167 | 81.885 | 23.6675 | 7 | 2.6854 | 0.0509 | -0.8382 | 6.6773 | 0.3754 | 1.1636 | -0.0725 | -0.0625 | 0.6675 | 0.6014 | -0.009 | -1.4196 | -0.0579 | 0.0457 | 0.0816 | 0.208 | 0.0123 | -0.162 | 0.1575 | 0.0639 | 0.4456 | -15.4404 | 89.6268 | 25.9164 | 8 | 8.3998 | -1.484 | 1.9304 | 7.6391 | -1.053 | 2.6649 | 0.0119 | 0.1232 | 0.7421 | -0.1862 | -0.0537 | -1.472 | -0.161 | 0.2974 | 0.0417 | 0.1765 | 0.0051 | 0.0485 | 0.184 | 0.1519 | 0.3828 | -16.4724 | 88.7275 | 17.3721 | 9 | 6.6504 | 0.1599 | 1.699 | 10.5909 | 0.3072 | 3.9841 | -0.0013 | 0.8081 | 0.5237 | -1.4478 | -0.1024 | -0.0343 | -0.1263 | -0.2316 | 0.1036 | 0.4087 | 0.0257 | 0.0549 | 0.3282 | 0.1558 | 0.18 | -23.91 | 84.5377 | 11.1361 | 10 | 1.321 | 0.9689 | -0.0653 | 11.7681 | -1.6278 | 3.9774 | 0.1412 | 0.7372 | 0.404 | -1.4478 | -0.1274 | 0.2599 | -0.2827 | 0.0016 | -0.0137 | 0.5576 | 0.0431 | -0.0549 | 0.3849 | 0.091 | 0.1194 | -28.5881 | 77.7807 | 7.8768 | 11 | 2.9686 | 3.1341 | 3.3993 | 5.5705 | 2.1874 | 4.7621 | 0.0474 | 0.2264 | 0.0377 | -0.3455 | -0.0435 | 0.1468 | 0.2436 | 0.0437 | -0.0038 | 0.2647 | 0.015 | -0.0287 | 0.252 | 0.0914 | 0.1149 | -28.9671 | 79.1515 | 16.3893 | 12 | 1.6822 | -0.1278 | 0.8446 | 6.9011 | 0.1773 | 2.9303 | -0.0663 | -0.5229 | 0.5901 | 1.2805 | -0.0234 | -0.477 | -0.0506 | -0.0274 | 0.0896 | 0.2843 | 0.0129 | -0.0757 | 0.1786 | 0.03 | 0.115 | -24.1843 | 86.7352 | 29.0961 | 13 | 2.9425 | -0.8591 | 1.5775 | 4.9523 | -1.8347 | 1.2479 | -0.0254 | -0.2964 | 0.0589 | 1.3123 | -0.0256 | -0.2185 | 0.2163 | -0.0389 | 0.0511 | 0.5553 | 0.0072 | -0.0513 | 0.2967 | 0.0332 | 0.0926 | -25.7366 | 81.7608 | 33.7268 | 14 | 2.7867 | 1.1578 | 2.8423 | 10.0214 | 1.2861 | 5.0962 | 0.0106 | -0.8306 | 0.2111 | 1.8241 | 0.0334 | -0.5133 | 0.0547 | 0.042 | -0.0439 | 0.5727 | -0.0031 | -0.1004 | 0.2992 | 0.097 | 0.1121 | -23.5636 | 74.3496 | 33.0322 | 15 | 4.7571 | 1.3741 | -1.3207 | 10.0882 | -0.5586 | 0.3746 | 0.0002 | -0.5179 | -0.0156 | 1.2692 | 0.0158 | -1.3565 | 0.1021 | 0.1366 | -0.0159 | 0.3214 | 0.0246 | -0.167 | 0.2047 | 0.0679 | 0.2804 | -16.9661 | 78.305 | 28.1653 | 16 | 5.8975 | 1.5639 | 0.806 | 6.7454 | -0.8546 | 0.2968 | 0.0451 | 0.3937 | -0.6475 | -0.2105 | -0.0274 | 0.1085 | 0.3726 | -0.1047 | -0.0177 | 0.2539 | 0.0005 | -0.0247 | 0.2257 | 0.0765 | 0.12 | -28.2996 | 70.1704 | 20.2985 | 17 | 2.311 | -2.7582 | 1.1216 | 7.2136 | 1.24 | 2.2463 | 0.0299 | 0.0299 | -0.4557 | 0.2405 | -0.0176 | -0.5081 | 0.2309 | -0.0486 | -0.0123 | 0.2783 | 0.0126 | -0.0522 | 0.2255 | 0.0846 | 0.1451 | -22.4693 | 69.8874 | 22.234 | 18 | 2.5955 | -0.2817 | 0.4531 | 8.3651 | -2.388 | 0.7354 | 0.0452 | 0.1563 | 0.1441 | -0.1501 | -0.0373 | -1.6111 | 0.1573 | 0.0524 | -0.008 | 0.1309 | 0.0212 | 0.0544 | 0.1542 | 0.1078 | 0.3907 | -13.0327 | 79.6516 | 17.8851 | 19 | 5.1478 | 1.1157 | -0.9162 | 6.0022 | 2.3429 | 1.2852 | 0.0454 | 0.733 | 0.4829 | -1.255 | -0.0589 | -0.9938 | -0.3127 | -0.1908 | 0.0136 | 0.3776 | 0.0353 | 0.2086 | 0.3065 | 0.134 | 0.2917 | -16.0889 | 79.5238 | 10.2211 | 20 | 4.0946 | -0.9188 | 1.1354 | 11.4915 | -1.1781 | 5.1964 | 0.0914 | 0.5059 | -0.4812 | -1.0873 | -0.073 | -0.6865 | 0.4525 | -0.0312 | -0.0184 | 0.33 | 0.0491 | 0.0846 | 0.2585 | 0.0478 | 0.1227 | -20.4176 | 71.176 | 11.5248 | 21 | 2.0971 | 0.2108 | -1.0994 | 4.8877 | -2.9656 | 2.2607 | 0.1637 | -0.8971 | -0.8302 | 2.3884 | 0.0533 | -1.2021 | 0.2089 | 0.0403 | -0.217 | 0.9962 | -0.0084 | -0.5207 | 0.3535 | 0.2853 | 0.7791 | -14.3353 | 51.4626 | 37.0056 | 22 | 3.5939 | -0.4852 | 0.0153 | 7.0221 | 0.2799 | 0.0115 | 0.2468 | -0.0961 | -0.675 | 0.7888 | 0.0473 | -2.3113 | 0.1478 | 0.1855 | -0.2941 | 0.378 | 0.059 | -0.3756 | 0.1766 | 0.0772 | 1.1668 | -5.7766 | 53.8456 | 26.2794 | 23 | 4.5651 | -0.973 | 1.66 | 8.9442 | -2.6351 | 1.1998 | 0.287 | 0.3526 | -1.0258 | 0.1249 | -0.0257 | -2.0543 | 0.2794 | 0.2088 | -0.2614 | 0.3306 | 0.0675 | -0.2661 | 0.1437 | 0.0262 | 1.1124 | -8.5124 | 47.9999 | 22.7662 | 24 | 2.2618 | -0.4438 | 1.8289 | 12.5333 | -0.9567 | 1.5836 | 0.3432 | 0.0927 | -1.1836 | 0.3343 | -0.0073 | -1.3341 | 0.353 | 0.0873 | -0.336 | 0.3529 | 0.0532 | -0.2707 | 0.1206 | 0.0286 | 1.0001 | -13.2095 | 43.4642 | 22.147 | 25 | 4.1575 | -1.9612 | 0.1814 | 5.7985 | -0.7916 | 0.9604 | 0.2446 | -0.093 | -1.1184 | 0.7358 | 0.0016 | -0.7242 | 0.3712 | -0.0071 | -0.2462 | 0.4092 | -0.0051 | -0.2316 | 0.1491 | 0.144 | 0.5908 | -19.6324 | 48.7451 | 26.3428 | 26 | 2.0018 | 2.7174 | 0.8649 | 10.9202 | 3.211 | 0.9493 | 0.1938 | -0.1205 | -0.5109 | 0.7767 | -0.0266 | -1.2453 | 0.1778 | -0.0266 | -0.1673 | 0.3366 | 0.0243 | -0.2204 | 0.1783 | 0.1039 | 0.492 | -14.56 | 59.7205 | 26.1231 | 27 | 5.6309 | -0.8784 | -1.4 | 7.581 | 0.8455 | 0.4011 | 0.0805 | -0.386 | -0.2912 | 1.1733 | 0.001 | -1.6011 | 0.1652 | 0.1853 | -0.0815 | 0.3913 | 0.0125 | -0.2521 | 0.2136 | 0.1016 | 0.3992 | -14.1999 | 68.9523 | 28.882 | 28 | 2.6909 | 0.7143 | 0.3845 | 4.5621 | 1.3666 | 0.4644 | 0.0792 | -0.3067 | -0.5555 | 1.4198 | 0.0449 | -0.7148 | 0.2534 | -0.0042 | -0.1242 | 0.7354 | -0.0161 | -0.2076 | 0.335 | 0.1887 | 0.2934 | -20.9935 | 62.4568 | 34.3362 | 29 | 4.159 | -0.8236 | 2.2227 | 5.7299 | -0.3432 | 3.0709 | 0.1414 | -0.6814 | -0.6404 | 2.0586 | 0.0447 | -0.1932 | 0.0611 | -0.1516 | -0.1862 | 0.9917 | -0.0523 | -0.1864 | 0.3827 | 0.3223 | 0.4742 | -23.6088 | 52.9268 | 37.3639 | 30 | 4.5214 | -0.8798 | 0.2767 | 8.7109 | -0.5482 | 3.5677 | 0.2627 | -0.6075 | -1.4318 | 1.6053 | -0.0248 | -0.2733 | 0.5972 | -0.3295 | -0.2378 | 0.6893 | -0.0311 | -0.2626 | 0.2344 | 0.2623 | 0.6375 | -21.5429 | 47.4466 | 32.1899 | 31 | 4.8247 | 0.5876 | 0.9379 | 9.9028 | -0.3161 | 1.1445 | 0.1812 | 0.0835 | -0.4111 | 0.5052 | 0.0008 | -2.1884 | 0.0943 | 0.199 | -0.182 | 0.281 | 0.049 | -0.2474 | 0.1685 | 0.0671 | 0.8386 | -7.895 | 61.1355 | 24.8009 | 32 | 3.055 | -0.4954 | -0.0212 | 6.3284 | -0.2499 | 0.0104 | 0.2351 | 0.4842 | -0.5986 | -0.5884 | -0.0401 | -1.6909 | 0.1947 | 0.0524 | -0.195 | 0.2665 | 0.0755 | 0.0471 | 0.2041 | -0.0228 | 0.7158 | -10.2779 | 58.155 | 15.6888 | 33 | 0.89 | 0.2053 | 0.2003 | 1.9035 | -0.3742 | 0.1403 | 0.2514 | 0.2913 | -0.8487 | -0.7027 | -0.0794 | -1.2058 | 0.4774 | 0.1737 | -0.172 | 0.2532 | 0.0616 | 0.053 | 0.1668 | -0.009 | 0.3436 | -15.8474 | 60.7366 | 14.0098 | 34 | 3.3295 | -0.1677 | 0.5224 | 6.9202 | -1.3067 | 0.32 | 0.1116 | 0.2214 | -0.4743 | 0.097 | 0.0034 | -0.7618 | 0.2787 | -0.186 | -0.115 | 0.2271 | 0.016 | -0.0838 | 0.159 | 0.0757 | 0.2463 | -18.1976 | 64.5938 | 22.2697 | 35 | 3.81 | 0.0327 | -0.2202 | 6.6353 | -1.7067 | 1.4326 | 0.2207 | 0.067 | -1.1418 | 0.2282 | -0.0189 | -0.4578 | 0.4356 | -0.0776 | -0.2019 | 0.2869 | 0.0104 | -0.1596 | 0.1259 | 0.0693 | 0.4708 | -21.1487 | 50.6853 | 21.9807 | 36 | 1.1967 | -3.3462 | 0.8541 | 9.4376 | -2.3577 | 0.621 | 0.3227 | 0.4124 | -1.2023 | -0.586 | -0.0636 | -0.7761 | 0.52 | 0.1066 | -0.2592 | 0.3369 | 0.0394 | -0.1718 | 0.138 | -0.0247 | 0.725 | -19.2588 | 45.1436 | 17.9908 | 37 | 0.3875 | -1.6154 | -0.1146 | 6.7403 | 0.478 | 0.0339 | 0.2345 | 0.2916 | -0.8584 | -0.3825 | -0.0518 | -0.1341 | 0.2144 | -0.0054 | -0.1826 | 0.2395 | 0.0097 | -0.0938 | 0.1333 | 0.0346 | 0.2792 | -24.6382 | 55.9282 | 18.6903 | 38 | 1.4654 | -0.2581 | -0.4994 | 4.8292 | 0.5607 | 0.24 | 0.1765 | -0.6027 | -0.6841 | 1.505 | -0.0356 | 0.2893 | 0.1957 | -0.1029 | -0.1409 | 0.5564 | -0.0405 | -0.0283 | 0.3007 | 0.1831 | 0.2497 | -27.6019 | 61.286 | 30.9039 | 39 | 4.2347 | -1.9083 | -0.8731 | 6.5677 | 2.3486 | 2.2753 | 0.1832 | -0.4362 | -0.5513 | 1.1614 | -0.0397 | 0.6786 | -0.0226 | -0.313 | -0.1436 | 0.4635 | -0.0585 | -0.0104 | 0.2343 | 0.1937 | 0.3658 | -30.4864 | 56.2363 | 28.8279 | 40 | 5.5871 | -4.7306 | 2.6043 | 10.4907 | 1.887 | 4.0046 | 0.2667 | 0.0172 | -1.4447 | 0.5609 | -0.1166 | 0.6222 | 0.6808 | -0.0071 | -0.1501 | 0.4113 | -0.0702 | -0.0827 | 0.1779 | 0.1794 | 0.6145 | -30.9196 | 48.3259 | 25.931 |
|
---|
精密化 TLSグループ | ID | Refine-ID | Refine TLS-ID | Auth asym-ID | Label asym-ID | Auth seq-ID | Label seq-ID |
---|
1 | X-RAY DIFFRACTION | 1 | AA2 - 4 | 2 - 4 | 2 | X-RAY DIFFRACTION | 2 | AA5 - 9 | 5 - 9 | 3 | X-RAY DIFFRACTION | 3 | AA10 - 15 | 10 - 15 | 4 | X-RAY DIFFRACTION | 4 | AA16 - 19 | 16 - 19 | 5 | X-RAY DIFFRACTION | 5 | AA20 - 23 | 20 - 23 | 6 | X-RAY DIFFRACTION | 6 | AA24 - 28 | 24 - 28 | 7 | X-RAY DIFFRACTION | 7 | AA29 - 35 | 29 - 35 | 8 | X-RAY DIFFRACTION | 8 | AA36 - 40 | 36 - 40 | 9 | X-RAY DIFFRACTION | 9 | AA41 - 47 | 41 - 47 | 10 | X-RAY DIFFRACTION | 10 | AA48 - 52 | 48 - 52 | 11 | X-RAY DIFFRACTION | 11 | AA53 - 56 | 53 - 56 | 12 | X-RAY DIFFRACTION | 12 | AA57 - 62 | 57 - 62 | 13 | X-RAY DIFFRACTION | 13 | AA63 - 67 | 63 - 67 | 14 | X-RAY DIFFRACTION | 14 | AA68 - 71 | 68 - 71 | 15 | X-RAY DIFFRACTION | 15 | AA72 - 79 | 72 - 79 | 16 | X-RAY DIFFRACTION | 16 | AA80 - 83 | 80 - 83 | 17 | X-RAY DIFFRACTION | 17 | AA84 - 90 | 84 - 90 | 18 | X-RAY DIFFRACTION | 18 | AA91 - 95 | 91 - 95 | 19 | X-RAY DIFFRACTION | 19 | AA96 - 99 | 96 - 99 | 20 | X-RAY DIFFRACTION | 20 | AA100 - 108 | 100 - 108 | 21 | X-RAY DIFFRACTION | 21 | BB2 - 5 | 2 - 5 | 22 | X-RAY DIFFRACTION | 22 | BB6 - 10 | 6 - 10 | 23 | X-RAY DIFFRACTION | 23 | BB11 - 15 | 11 - 15 | 24 | X-RAY DIFFRACTION | 24 | BB16 - 20 | 16 - 20 | 25 | X-RAY DIFFRACTION | 25 | BB21 - 24 | 21 - 24 | 26 | X-RAY DIFFRACTION | 26 | BB25 - 28 | 25 - 28 | 27 | X-RAY DIFFRACTION | 27 | BB29 - 36 | 29 - 36 | 28 | X-RAY DIFFRACTION | 28 | BB37 - 42 | 37 - 42 | 29 | X-RAY DIFFRACTION | 29 | BB43 - 49 | 43 - 49 | 30 | X-RAY DIFFRACTION | 30 | BB50 - 56 | 50 - 56 | 31 | X-RAY DIFFRACTION | 31 | BB57 - 64 | 57 - 64 | 32 | X-RAY DIFFRACTION | 32 | BB65 - 69 | 65 - 69 | 33 | X-RAY DIFFRACTION | 33 | BB70 - 73 | 70 - 73 | 34 | X-RAY DIFFRACTION | 34 | BB74 - 77 | 74 - 77 | 35 | X-RAY DIFFRACTION | 35 | BB78 - 82 | 78 - 82 | |
| | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | |
|
---|