9VUR
Crystal Structure of TEAD2 in a covalent complex with LC-TEAD01
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL18U1 |
| Synchrotron site | SSRF |
| Beamline | BL18U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2025-04-12 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.97853 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 122.916, 61.552, 79.726 |
| Unit cell angles | 90.00, 117.52, 90.00 |
Refinement procedure
| Resolution | 70.700 - 2.660 |
| R-factor | 0.20997 |
| Rwork | 0.208 |
| R-free | 0.25628 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.178 |
| Data reduction software | autoPROC |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0415) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 70.700 | 2.800 |
| High resolution limit [Å] | 2.660 | 2.660 |
| Rmerge | 0.169 | 0.792 |
| Rmeas | 0.188 | 0.883 |
| Rpim | 0.081 | 0.383 |
| Total number of observations | 74613 | 10732 |
| Number of reflections | 15111 | 2183 |
| <I/σ(I)> | 7.5 | 2.3 |
| Completeness [%] | 98.4 | |
| Redundancy | 4.9 | 4.9 |
| CC(1/2) | 0.990 | 0.752 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | Sodium Formate 2.0M HEPES pH 7.2 - 8.0 |
