Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL02U1 |
| Synchrotron site | SSRF |
| Beamline | BL02U1 |
| Temperature [K] | 80 |
| Detector technology | CCD |
| Collection date | 2024-04-13 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.97918 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 212.436, 49.778, 66.953 |
| Unit cell angles | 90.00, 107.50, 90.00 |
Refinement procedure
| Resolution | 50.650 - 1.880 |
| R-factor | 0.1727 |
| Rwork | 0.171 |
| R-free | 0.20470 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.109 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 101.300 | 1.950 |
| High resolution limit [Å] | 1.880 | 1.880 |
| Rmerge | 0.109 | 0.730 |
| Number of reflections | 54565 | 7923 |
| <I/σ(I)> | 9.1 | 2.7 |
| Completeness [%] | 99.9 | 99.15 |
| Redundancy | 4.1 | 3.3 |
| CC(1/2) | 0.993 | 0.549 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 277 | 18% (w/v) PEG 8000, 0.2 M LiSO4, and 0.1 M MES, pH 6.5 |
