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9RM2

BKPyV VP1 IN COMPLEX WITH 319C07-FAB

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X10SA
Synchrotron siteSLS
BeamlineX10SA
Temperature [K]100
Detector technologyPIXEL
Collection date2023-06-07
DetectorDECTRIS EIGER2 S 16M
Wavelength(s)0.9999
Spacegroup nameP 1 21 1
Unit cell lengths109.349, 172.078, 113.144
Unit cell angles90.00, 97.64, 90.00
Refinement procedure
Resolution91.870 - 1.960
R-factor0.18892
Rwork0.187
R-free0.21819
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.004
RMSD bond angle1.361
Data reduction softwareautoPROC
Data scaling softwareautoPROC ((Version 1.1.7))
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0267)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]91.8701.991
High resolution limit [Å]1.9571.957
Rmerge0.0941.220
Number of reflections295460295460
<I/σ(I)>8.51.3
Completeness [%]99.498.7
Redundancy4.44.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP2930.1 M MIB buffer pH 4.75, 21% (w/v) PEG 1500

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