9RM2
BKPyV VP1 IN COMPLEX WITH 319C07-FAB
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-06-07 |
Detector | DECTRIS EIGER2 S 16M |
Wavelength(s) | 0.9999 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 109.349, 172.078, 113.144 |
Unit cell angles | 90.00, 97.64, 90.00 |
Refinement procedure
Resolution | 91.870 - 1.960 |
R-factor | 0.18892 |
Rwork | 0.187 |
R-free | 0.21819 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 1.361 |
Data reduction software | autoPROC |
Data scaling software | autoPROC ((Version 1.1.7)) |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 91.870 | 1.991 |
High resolution limit [Å] | 1.957 | 1.957 |
Rmerge | 0.094 | 1.220 |
Number of reflections | 295460 | 295460 |
<I/σ(I)> | 8.5 | 1.3 |
Completeness [%] | 99.4 | 98.7 |
Redundancy | 4.4 | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M MIB buffer pH 4.75, 21% (w/v) PEG 1500 |