Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-01-11 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.000020 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 41.850, 62.540, 101.197 |
| Unit cell angles | 90.00, 93.71, 90.00 |
Refinement procedure
| Resolution | 41.800 - 1.800 |
| R-factor | 0.23868 |
| Rwork | 0.236 |
| R-free | 0.28935 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.761 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0425) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 41.800 | 1.840 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Number of reflections | 47991 | 2873 |
| <I/σ(I)> | 16.2 | 2.9 |
| Completeness [%] | 99.0 | |
| Redundancy | 7 | |
| CC(1/2) | 0.999 | 0.885 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 277.15 | 31% PEG 3350, 0.2M MgCl2, 0.1M MES pH5.5. |
