Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 HF |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2018-11-18 |
| Detector | RIGAKU RAXIS IV++ |
| Wavelength(s) | 1.542 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 136.613, 141.246, 87.350 |
| Unit cell angles | 90.00, 126.72, 90.00 |
Refinement procedure
| Resolution | 49.720 - 2.430 |
| R-factor | 0.2478 |
| Rwork | 0.245 |
| R-free | 0.29500 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.549 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.720 | 2.517 |
| High resolution limit [Å] | 2.430 | 2.430 |
| Rmerge | 0.193 | 0.897 |
| Rmeas | 0.227 | 1.055 |
| Rpim | 0.118 | 0.550 |
| Number of reflections | 49871 | 4938 |
| <I/σ(I)> | 4.04 | 1.1 |
| Completeness [%] | 99.7 | |
| Redundancy | 3.7 | |
| CC(1/2) | 0.987 | 0.688 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5 | 293.15 | 100 mM sodium acetate, 2.0M ammonium sulfate |
