Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-03-18 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.0 |
| Spacegroup name | F 2 3 |
| Unit cell lengths | 177.590, 177.590, 177.590 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 25.000 - 2.500 |
| R-factor | 0.202 |
| Rwork | 0.201 |
| R-free | 0.22000 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.060 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.7) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 25.000 | 10.000 | 2.570 |
| High resolution limit [Å] | 2.500 | 10.000 | 2.500 |
| Rmerge | 0.193 | 0.050 | 1.800 |
| Rmeas | 0.198 | 0.052 | 1.000 |
| Number of reflections | 16143 | 193 | 1178 |
| <I/σ(I)> | 14.41 | ||
| Completeness [%] | 99.9 | ||
| Redundancy | 20 | ||
| CC(1/2) | 0.999 | 0.999 | 0.694 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 294 | 10 % PEG8000, LITHIUM SULPHATE 0.5M |
