Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-02-10 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 1.00003231311 |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 145.160, 145.160, 145.160 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 72.690 - 2.060 |
| R-factor | 0.1692 |
| Rwork | 0.168 |
| R-free | 0.19650 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.571 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 72.690 | 2.092 |
| High resolution limit [Å] | 2.057 | 2.057 |
| Number of reflections | 802325 | 1561 |
| <I/σ(I)> | 22.3 | |
| Completeness [%] | 100.0 | |
| Redundancy | 25.3 | |
| CC(1/2) | 1.000 | 0.559 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | sodium tartrate, sodium acetate, ammonium chloride |
