9F82

Arbitrium receptor from ATCC13952 phage in complex with GVVRGA peptide

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALBA BEAMLINE XALOC
Synchrotron site	ALBA
Beamline	XALOC
Temperature [K]	80
Detector technology	PIXEL
Collection date	2020-09-17
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97918
Spacegroup name	P 1 21 1
Unit cell lengths	67.343, 82.959, 146.860
Unit cell angles	90.00, 90.88, 90.00

Refinement procedure

Resolution	146.840 - 3.100
R-factor	0.23053
Rwork	0.228
R-free	0.27694
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	MOLREP
Refinement software	REFMAC (5.8.0425)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	146.840	3.290
High resolution limit [Å]	3.100	3.100
Number of reflections	29584	4750
<I/σ(I)>	8.7
Completeness [%]	99.8
Redundancy	6.7
CC(1/2)	0.994	0.920

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		294	30% PEG 3000 0.1M CHES pH 9.5