Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-06-09 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.0000 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 90.813, 90.813, 122.738 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 78.650 - 1.490 |
| R-factor | 0.12703 |
| Rwork | 0.126 |
| R-free | 0.15573 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.018 |
| RMSD bond angle | 1.855 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 78.650 | 1.740 |
| High resolution limit [Å] | 1.490 | 1.490 |
| Number of reflections | 95535 | 35297 |
| <I/σ(I)> | 13.75 | 3.01 |
| Completeness [%] | 99.6 | 99.9 |
| Redundancy | 3.5 | 3.5 |
| CC(1/2) | 0.999 | 0.831 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | 0.10 M NaAcetate pH4.8, 2.0 M (NH4)2SO4 30 % Glycerol |
