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9CP0

Crystal structure of the porcine astrovirus 4 capsid spike domain

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 5.0.1
Synchrotron siteALS
Beamline5.0.1
Temperature [K]100
Detector technologyPIXEL
Collection date2023-11-11
DetectorDECTRIS PILATUS3 2M
Wavelength(s)0.97
Spacegroup nameP 1
Unit cell lengths46.386, 66.211, 87.752
Unit cell angles74.54, 81.67, 78.61
Refinement procedure
Resolution39.780 - 1.850
R-factor0.3175
Rwork0.316
R-free0.36170
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.004
RMSD bond angle0.743
Data reduction softwareDIALS
Data scaling softwareDIALS
Phasing softwarePHASER
Refinement softwarePHENIX (1.20.1_4487)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]39.7801.880
High resolution limit [Å]1.8501.850
Number of reflections805263920
<I/σ(I)>8.12.1
Completeness [%]96.1
Redundancy3.2
CC(1/2)0.9840.814
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP72950.2 M calcium acetate hydrate, 0.1 M Tris-Cl pH 7, and 12% PEG 3000

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