9BVT
RNA Pol II - High Mn(+2) concentration
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-1 |
Synchrotron site | SSRL |
Beamline | BL12-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-04-21 |
Detector | DECTRIS PILATUS 12M |
Wavelength(s) | 0.9794 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 221.190, 393.970, 283.280 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.250 - 3.400 |
R-factor | 0.2215 |
Rwork | 0.220 |
R-free | 0.24870 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.670 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 197.000 | 3.650 |
High resolution limit [Å] | 3.350 | 3.350 |
Number of reflections | 175204 | 10487 |
<I/σ(I)> | 6.2 | |
Completeness [%] | 99.0 | |
Redundancy | 4.5 | |
CC(1/2) | 0.920 | 0.280 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | Tacsimate Hepes |