Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-05-11 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.99 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 60.685, 74.380, 90.109 |
| Unit cell angles | 90.00, 90.10, 90.00 |
Refinement procedure
| Resolution | 50.427 - 2.462 |
| Rwork | 0.302 |
| R-free | 0.36800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.693 |
| Data reduction software | autoPROC |
| Data scaling software | autoPROC |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.427 | 2.560 |
| High resolution limit [Å] | 2.460 | 2.460 |
| Number of reflections | 24473 | 1326 |
| <I/σ(I)> | 3 | |
| Completeness [%] | 83.6 | |
| Redundancy | 3.1 | |
| CC(1/2) | 0.978 | 0.500 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291.15 | 20% PEG 4000, 5% iso-Propanol, 0.1 M Na Citrate |
