9GC7
Mineralocorticoid receptor in complex with acylurea antagonists.
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-11-19 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.992 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 48.472, 77.789, 78.055 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 41.180 - 1.460 |
| R-factor | 0.1869 |
| Rwork | 0.186 |
| R-free | 0.20990 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.030 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | BUSTER (2.11.8) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 41.180 | 1.510 |
| High resolution limit [Å] | 1.460 | 1.460 |
| Rpim | 0.493 | |
| Number of reflections | 51196 | 4331 |
| <I/σ(I)> | 18.2 | 1.5 |
| Completeness [%] | 98.6 | |
| Redundancy | 6.3 | |
| CC(1/2) | 0.999 | 0.571 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 0.9 M AMS 0.1 M CHES pH 9.5 +10% Morpheus G8 |
