9EXX
Crystal structure of the PWWP1 domain of NSD2 bound by compound 18.
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-12-02 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97950 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.149, 54.939, 149.623 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 74.810 - 1.943 |
R-factor | 0.2344 |
Rwork | 0.233 |
R-free | 0.26510 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.920 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.8) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 74.812 | 2.131 |
High resolution limit [Å] | 1.943 | 1.943 |
Number of reflections | 21582 | 1081 |
<I/σ(I)> | 17.6 | |
Completeness [%] | 93.1 | |
Redundancy | 6.6 | |
CC(1/2) | 0.999 | 0.754 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 30 % ethanol |