9EM6
OPR3 variant Y364P in its dimeric form obtained without ammonium sulfate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2024-02-08 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 0.87 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 58.005, 90.053, 81.241 |
Unit cell angles | 90.00, 109.13, 90.00 |
Refinement procedure
Resolution | 46.810 - 1.720 |
R-factor | 0.1815 |
Rwork | 0.180 |
R-free | 0.21470 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 0.884 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.21_5207) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.810 | 1.740 |
High resolution limit [Å] | 1.720 | 1.720 |
Rpim | 0.036 | 0.980 |
Number of reflections | 81190 | 1595 |
<I/σ(I)> | 10.14 | |
Completeness [%] | 96.9 | |
Redundancy | 6.6 | |
CC(1/2) | 0.990 | 0.290 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 0.1 M Tris-HCl (7.5), 50 mM sodium tartrate, 8-16% PEG8000 |