Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-02-07 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.99977 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 214.362, 50.260, 64.906 |
| Unit cell angles | 90.00, 107.00, 90.00 |
Refinement procedure
| Resolution | 102.500 - 2.790 |
| R-factor | 0.2421 |
| Rwork | 0.240 |
| R-free | 0.28790 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.366 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | REFMAC |
| Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 102.500 | 3.040 |
| High resolution limit [Å] | 2.790 | 2.790 |
| Rmerge | 0.046 | 0.446 |
| Number of reflections | 16388 | 3721 |
| <I/σ(I)> | 19.3 | |
| Completeness [%] | 97.5 | 98.9 |
| Redundancy | 2.8 | 2.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 18% w/v PEG 3350, 0.2M (NH4)2 TARTRATE |
