8YHL

The Crystal Structure of Tgf-Beta Type I Receptor (Alk5) from Biortus

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08B1-1
Synchrotron site	CLSI
Beamline	08B1-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-02-18
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	1.18067
Spacegroup name	P 21 21 21
Unit cell lengths	41.813, 77.464, 89.524
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.762 - 1.470
Rwork	0.163
R-free	0.19320
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.012
RMSD bond angle	1.726
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	REFMAC (5.8.0267)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.760	1.500
High resolution limit [Å]	1.470	1.470
Number of reflections	50369	2526
<I/σ(I)>	18.3
Completeness [%]	100.0
Redundancy	6.4
CC(1/2)	0.999	0.683

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.1M MgAC2, 0.1M MES pH6.5, 10% PEG10,000