Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL18U1 |
| Synchrotron site | SSRF |
| Beamline | BL18U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-01-05 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.9785 |
| Spacegroup name | P 63 |
| Unit cell lengths | 82.415, 82.415, 63.472 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 47.430 - 2.500 |
| Rwork | 0.226 |
| R-free | 0.29070 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.744 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0352) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.430 | 2.600 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Number of reflections | 8584 | 984 |
| <I/σ(I)> | 9.2 | |
| Completeness [%] | 99.9 | |
| Redundancy | 7.2 | |
| CC(1/2) | 0.980 | 0.699 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2M Ammonium phosphate monobasic, 0.1M Tris (8.3 8.7), 40% MPD |
