Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS-II BEAMLINE 19-ID |
| Synchrotron site | NSLS-II |
| Beamline | 19-ID |
| Temperature [K] | 80 |
| Detector technology | PIXEL |
| Collection date | 2022-07-22 |
| Detector | DECTRIS EIGER2 XE 9M |
| Wavelength(s) | 1 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 58.011, 64.654, 138.729 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 43.178 - 2.100 |
| R-factor | 0.2726 |
| Rwork | 0.271 |
| R-free | 0.29980 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.303 |
| Data reduction software | XDS |
| Data scaling software | pointless |
| Phasing software | BUCCANEER |
| Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.290 | 2.180 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Rmerge | 0.125 | 0.217 |
| Number of reflections | 31260 | 2538 |
| <I/σ(I)> | 15.1 | |
| Completeness [%] | 99.3 | |
| Redundancy | 6.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 2.0 MgSO4, 0.1 M MES pH 6.5 |
