8TUD
IgG1 Fc Heterodimer combYSelect2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-12-10 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.014, 79.685, 139.308 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.360 - 3.000 |
R-factor | 0.2063 |
Rwork | 0.198 |
R-free | 0.28520 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.221 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PDB-REDO |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.360 | 3.108 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.453 | 3.074 |
Rmeas | 0.474 | 3.221 |
Rpim | 0.137 | 0.949 |
Number of reflections | 11350 | 993 |
<I/σ(I)> | 18.5 | 2.7 |
Completeness [%] | 96.9 | 86.27 |
Redundancy | 11.5 | 10.7 |
CC(1/2) | 0.964 | 0.628 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 292 | 0.1M Bis Tris pH 6.5 and 29% PEG MME 2000 |