Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

8T09

Co-crystal structure of KRIT1 with a 1-hydroxy 2-naphthaldehyde derivative (6-ethynyl-2-hydroxy-1-naphthaldehyde)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 8.2.2
Synchrotron siteALS
Beamline8.2.2
Temperature [K]100
Detector technologyCCD
Collection date2021-10-22
DetectorADSC QUANTUM 315r
Wavelength(s)0.987
Spacegroup nameP 1 21 1
Unit cell lengths57.530, 77.922, 58.711
Unit cell angles90.00, 91.54, 90.00
Refinement procedure
Resolution46.880 - 2.150
R-factor0.2029
Rwork0.201
R-free0.24720
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.003
RMSD bond angle0.553
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwarePHENIX (1.19.2_4158)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]58.7002.190
High resolution limit [Å]2.1002.150
Rmerge0.0630.067
Number of reflections28217772
<I/σ(I)>13.85
Completeness [%]91.8
Redundancy4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP29320% PEG 3350, 100mM Tris, pH 8.5, 100 mM KCl

223166

PDB entries from 2024-07-31

PDB statisticsPDBj update infoContact PDBjnumon