8RD7
HUWE1 WWE domain in complex with ADP-ribose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-09-25 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.999870 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 62.883, 62.883, 231.245 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.460 - 1.310 |
R-factor | 0.1491 |
Rwork | 0.148 |
R-free | 0.17710 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond angle | 18.393 |
Data reduction software | XDS (Jan 31, 202) |
Data scaling software | autoPROC (1.1.7) |
Phasing software | PHASER |
Refinement software | PHENIX ((1.21_5207: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.679 | 1.437 |
High resolution limit [Å] | 1.310 | 1.313 |
Rmerge | 0.057 | 1.544 |
Number of reflections | 87488 | 4372 |
<I/σ(I)> | 20.5 | 1.5 |
Completeness [%] | 78.3 | 16.7 |
Redundancy | 12.9 | 12.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 278 | 0.1 M Na Acetate pH 4.83, 2.9 M NaCl |